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Photolysis-ion chromatographic determination of N-nitrosodiethylamine

机译:Photolysis-ion色谱测定

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摘要

Photolysis-Griess reaction (PG) method, as a cost-effective spectrophotometry, is widely used in food enterprises for determination of nitrosamines such as N-nitrosodiethylamine (NDEA). The PG method was conducted based on the amount of photo-produced nitrite ions. Results of this research showed the possible errors of the PG method, since photolysis of NDEA not only generated nitrite, but also nitrate ions. The sum of the concentrations of the two photo-produced ions was found equivalent to the initial NDEA concentration before photolysis. Based on this finding, a photolysis-ion chromatography method was established with good precision and accuracy.
机译:Photolysis-Griess反应(PG)方法,作为一个具有成本效益的分光光度法,被广泛使用在食品企业的决心亚硝胺等N-nitrosodiethylamine(NDEA)。photo-produced亚硝酸盐离子。本研究显示的可能的错误PG方法,因为不仅NDEA光解生成亚硝酸盐,硝酸盐离子。两个photo-produced的浓度相当于初始NDEA离子被发现浓度在光解。发现,一个photolysis-ion色谱方法建立了具有良好的精密度和准确度。

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