Simultaneous Determination of Vitamin D_3 and K_1 in Infant Formula by Column-switching High Performance Liquid Chromatography with UV Detection

Byung-Man Kwak; Jang-Hyuk Ahn; Chi-Hoon Chang

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Simultaneous Determination of Vitamin D_3 and K_1 in Infant Formula by Column-switching High Performance Liquid Chromatography with UV Detection

机译：色谱柱切换高效液相色谱-紫外检测法同时测定婴儿配方食品中的维生素D_3和K_1

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摘要

Rapid and simple method was developed for simultaneous determination of vitamins D_3 and K_1 contents in infant formula. Contents of vitamins D_3 and K_1, extracted by column-switching HPLC with reversed phase column using enzymatic hydrolysis and organic solvent, in CRM determined by developed method were within certified ranges of standard values.

机译：建立了一种快速简便的方法，可同时测定婴儿配方食品中维生素D_3和K_1的含量。通过开发的方法测定的CRM中，采用酶促水解和有机溶剂的反相色谱柱切换HPLC提取的维生素D_3和K_1的含量在标准值的认可范围内。

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《Korean Journal of Food Science and Technology》 |2005年第6期|共4页
作者
Byung-Man Kwak; Jang-Hyuk Ahn; Chi-Hoon Chang;
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正文语种 kor
中图分类食品工业;
关键词
enzymatic hydrolysis extraction; column-switching HPLC; simultaneous determination;

机译：酶解萃取柱切换HPLC同时测定;

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专利

1. Simultaneous Determination of Vitamin D_3 and K_1 in Infant Formula by Column-switching High Performance Liquid Chromatography with UV Detection [J] . Byung-Man Kwak, Jang-Hyuk Ahn, Chi-Hoon Chang Korean Journal of Food Science and Technology . 2005,第6期

机译：色谱柱切换高效液相色谱-紫外检测法同时测定婴儿配方食品中的维生素D_3和K_1
2. Determination of vitamin B12 in infant formula and adult nutritionals by liquid chromatography/UV detection with immunoaffinity extraction: First Action 2011.08. [J] . Campos-Gimenez E, Fontannaz P, Trisconi M. J, Journal of AOAC International . 2012,第2期

机译：液相色谱/紫外检测-免疫亲和萃取法测定婴儿配方食品和成人营养食品中的维生素B12：First Action 2011.08。
3. Rapid determination of vitamin D_3 in milk-based infant formulas by liquid chromatography-tandem mass spectrometry [J] . Byung-Man Kwak, In-Seek Jeong, Moon-Seok Lee, Food Chemistry . 2014,第deca15期

机译：液相色谱-串联质谱法快速测定乳基婴儿配方食品中的维生素D_3
4. Development and Validation of a Liquid Chromatography-Tandem Mass Spectrometry for the Simultaneous Determination of B Group Vitamins in Infant Formula [C] . Joon Hyuk Suh, Byung Kyu Lee, Jeong-Rok Youm, American Society for Mass Spectrometry Conference on Mass Spectrometry and Allied Topics . 2009

机译：液相色谱 - 串联质谱法同时测定婴幼儿配方液中B群维生素的发展与验证
5. Simultaneous determination of Vitamins A, D3, E, and K1 in Micelle Emulsion by high performance liquid chromatography. [D] . Lin, Yi-Chun. 2011

机译：高效液相色谱法同时测定胶束乳液中的维生素A，D3，E和K1。
6. Simultaneous Determination of Isoniazid Pyrazinamide and Rifampin in Human Plasma by High-performance Liquid Chromatography and UV Detection [O] . Behnam Dasht Bozorg, Ali Goodarzi, Fanak Fahimi, 2019

机译：高效液相色谱和紫外检测同时测定人血浆中的异烟肼吡嗪酰胺和利福平
7. Determination of vitamin D3 and 25-hydroxyvitamin D3 in sera by column-switching high performance liquid chromatography with fluorescence detection. [O] . Tetsuharu IWATA, Masatoshi YAMAGUCHI, Hiroshi HANAZONO, 1990

机译：荧光检测柱切换高效液相色谱法测定血清中维生素D3和25-羟基乙多二胺D3。
8. Method 532: Determination of Phenylurea Compounds in Drinking Water by Solid Phase Extraction and High Performance Liquid Chromatography with UV Detection. Revision 1.0. [R] . Bassett, M. V., Wendelken, S. C., Dattilio, T. A., 2000

机译：方法532：固相萃取和高效液相色谱 - 紫外检测法测定饮用水中的苯基脲类化合物。修订版1.0。

Simultaneous Determination of Vitamin D_3 and K_1 in Infant Formula by Column-switching High Performance Liquid Chromatography with UV Detection

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