New ionic cobalt(III) complexes based on the N, N-bis(2-pyrazinecarboxamide)-1,2-benzene ligand: application to the formation of organic carbonates from epoxides and CO2

Adolph Michael; Zevaco Thomas A.; Altesleben Christiane; Staudt Simone; Walter Olaf; Dinjus Eckhard

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New ionic cobalt(III) complexes based on the N, N-bis(2-pyrazinecarboxamide)-1,2-benzene ligand: application to the formation of organic carbonates from epoxides and CO2

机译：基于N，N-双（2-吡嗪甲酰胺）-1,2-苯配体的新型离子钴（III）配合物：在环氧化物和CO2形成有机碳酸盐中的应用

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In this contribution, we report a further development within an "open'' N-4-ligand class obtained via condensation of 1,2-ortho-phenylene diamine with nitrogen-containing carboxylic acids. N, N-Bis(2-pyrazinecarboxamide)-1, 2-benzene reacted with different cobalt precursors to form new ionic Co(III) complexes in good yields. These compounds were successfully tested as potential catalysts for the coupling of epoxides with carbon dioxide.

机译：在此贡献中，我们报告了通过将1,2-邻苯二胺与含氮羧酸缩合而获得的“开放” N-4-配体类别中的进一步发展N，N-双（2-吡嗪甲酰胺） -1，2-苯与不同的钴前体反应生成高收率的新型离子型Co（III）络合物，已成功测试了这些化合物作为环氧化物与二氧化碳偶联的潜在催化剂。

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《New Journal of Chemistry》 |2015年第12期|共8页
作者
Adolph Michael; Zevaco Thomas A.; Altesleben Christiane; Staudt Simone; Walter Olaf; Dinjus Eckhard;
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1. New ionic cobalt(III) complexes based on the N, N-bis(2-pyrazinecarboxamide)-1,2-benzene ligand: application to the formation of organic carbonates from epoxides and CO2 [J] . Adolph Michael, Zevaco Thomas A., Altesleben Christiane, New Journal of Chemistry . 2015,第12期

机译：基于N，N-双（2-吡嗪甲酰胺）-1,2-苯配体的新型离子钴（III）配合物：在环氧化物和CO2形成有机碳酸盐中的应用
2. Synthesis, Redox Properties, and EPR Spectroscopy of Manganese(III) Complexes of the Ligand N,N-Bis(2-hydroxybenzyl)-N'-2-hydroxybenzylidene-1,2-diaminoethane: Formation of Mononuclear, Dinuclear, and Even Higher Nuclearity Complexes [J] . Heimo Schmitt, Reiner Lomoth, Ann Magnuson, Chemistry: A European journal . 2002,第16期

机译：N，N-双（2-羟基苄基）-N'-2-羟基苄叉基-1,2-二氨基乙烷配体的锰（III）配合物的合成，氧化还原性质和EPR光谱：单核，双核甚至更高价的形成核复合体
3. Iron(III) N,N-Dialkylcarbamate-Catalyzed Formation of Cyclic Carbonates from CO2 and Epoxides under Ambient Conditions by Dynamic CO2 Trapping as Carbamato Ligands [J] . Bresciani Giulio, Bortoluzzi Marco, Marchetti Fabio, ChemSusChem . 2018,第16期

机译：通过动态CO2捕获作为氨基甲酰胺配体，在环境条件下，熨斗（III）N，N-二烷基氨基酯催化在CO 2和环氧中形成的环碳酸酯的形成
4. 1,2-Migration of Aryl Groups on Silyl Ligands:Formation and Properties of Silylenetungusten Complexes Stabilized by an External Base [C] . Eiji Suzuki, Masaaki Okazaki, Hiromi Tobita Symposium on Organometallic Chemistry . 2004

机译：在甲硅烷基配体上的1,2-芳基偏移：由外部底座稳定的Silylenetuncusten复合物的形成和性质
5. MANGANESE(II) AND COBALT(III) COMPLEXES OF MULTIDENTATE LIGANDS: I. MANGANESE(II) COMPLEXES OF A MACROCYCLIC PENTADENTATE LIGAND. II. COBALT(III) COMPLEXES OF LINEAR TETRAMINE LIGANDS. [D] . HAMILTON, HOBART GORDON, JR. 1968

机译：多齿配体的锰（II）和钴（III）配合物：I.大环戊二烯配体的锰（II）配合物。二。线性叔丁胺配体的钴（III）配合物。
6. Cyclic Carbonate Formation from Epoxides and CO2 Catalyzedby Sustainable Alkali Halide–Glycol Complexes:A DFT Study to Elucidate Reaction Mechanism and Catalytic Activity [O] . Valeria Butera, Hermann Detz 2020

机译：环氧化物和CO2催化的环状碳酸盐形成通过可持续的碱卤化物 - 乙二醇配合物：阐明反应机制和催化活性的DFT研究
7. Cobalt(III) Complexes with Tripodlike Quadridentate Ligands. II. Preparations, Absorption Spectra and Circular Dichroism of (Amino carboxylato or 1,2-diamine)N,N-bis(2-aminoethyl)glycinatocobalt(III) Complexes [O] . Keiji Akamatsu, Takashi Komorita, Yoichi Shimura 1982

机译：钴（III）复合物与三脚架Quadri identate配体。 II。（氨基羧酸盐或1,2-二胺）N，N-双（2-氨基乙基）甘油酸钴（III）复合物的制备，吸收光谱和圆形二色性
8. Solution-Solid State Conformational Dependence in a Rigid-Ligand Lanthanide Complex. Preparation and Structure of Sodium(Diaquobis(Benzene-1,2-Dioxydiacetato)Lanthanate(III)) Tetrahydrate [R] . Kerfoot, H. B., Choppin, G. R., Kistenmacher, T. J. 1978

机译：刚 - 配体镧系元素配合物中溶液 - 固态构象依赖性。钠（Diaquobis（Benzene-1,2-Dioxydiacecetato）Lanthanate（III））四水合物的制备和结构

New ionic cobalt(III) complexes based on the N, N-bis(2-pyrazinecarboxamide)-1,2-benzene ligand: application to the formation of organic carbonates from epoxides and CO2

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