Expedient and efficient one pot synthesis of trifluoroethyl ethers from metal free 2,4,6-tris-(2,2,2-trifluoro-ethoxy)-[1,3,5] triazene

Mangawa Shrawan Kumar; Sharma Chiranjeev; Singh Ashawani Kumar; Awasthi Satish K.

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Expedient and efficient one pot synthesis of trifluoroethyl ethers from metal free 2,4,6-tris-(2,2,2-trifluoro-ethoxy)-[1,3,5] triazene

机译：从无金属的2,4,6-三-（2,2,2-三氟乙氧基）-[1,3,5]三叠氮烯中方便，高效地一锅合成三氟乙基醚

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An efficient synthesis of fluorinated alkyl and aryl ethers was achieved by the use of s-triazene derived fluorinated reagent 2,4,6-tris-(2,2,2-trifluoro-ethoxy)-[1,3,5] triazene (TriTFET). The procedure offers a very attractive alternative for the synthesis of fluorinated motifs that are found in various bioactive molecules. Moreover, TriTFET is a synthetic non-toxic, non-ozone depleting and stable reagent. All compounds were characterized by H-1, C-13 and F-19 NMR.

机译：使用s-三氮烯衍生的氟化试剂2,4,6-tris-（2,2,2-三氟乙氧基）-[1,3,5]三氮烯（ TriTFET）。该方法为合成各种生物活性分子中的氟化基序提供了非常有吸引力的替代方法。而且，TriTFET是一种合成的无毒，无臭氧消耗且稳定的试剂。所有化合物均通过H-1，C-13和F-19 NMR表征。

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《RSC Advances》 |2015年第44期|共4页
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Mangawa Shrawan Kumar; Sharma Chiranjeev; Singh Ashawani Kumar; Awasthi Satish K.;
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1. Expedient and efficient one pot synthesis of trifluoroethyl ethers from metal free 2,4,6-tris-(2,2,2-trifluoro-ethoxy)-[1,3,5] triazene [J] . Mangawa Shrawan Kumar, Sharma Chiranjeev, Singh Ashawani Kumar, RSC Advances . 2015,第44期

机译：从无金属的2,4,6-三-（2,2,2-三氟乙氧基）-[1,3,5]三叠氮烯中方便，高效地一锅合成三氟乙基醚
2. Synthesis and crystal structure of [Pb(trz)(tfpb)(H2O)]: a lead(II) complex containing 2,4,6-tris(2-pyridyl)-1,3,5-triazine and 4,4,4-trifluoro-1-phenyl-1,3-butandionate [J] . Marandi F, Asghari N, Gorbanloo M, Zeitschrift fur Anorganische und Allgemeine Chemie . 2007,第4期

机译：[Pb（trz）（tfpb）（H2O）]的合成和晶体结构：含2,4,6-三（2-吡啶基）-1,3,5-三嗪和4,4， 4-三氟-1-苯基-1,3-丁酸
3. Diaqua(trifluoroacetato-κ2O,O′)[2,4,6-tri-2-pyridyl-1,3,5-triazine-κ3N2,N1,N6]manganese(II) trifluoroacetate [J] . Lo K.M., Ng S.W. Acta Crystallographica Section E: Crystallographic Communications . 2009,第5期

机译：Diaqua（trifluoroacetato-κ2O，O'）[2,4,6-tri-2-pyridyl-1,3,5-triazine-κ3N2，N1，N6]三氟乙酸锰（II）
4. Electrosynthesis of Metal-Organic Frameworks (MOFs)Based on Nickel(II) and Benzene 1,3,5-Tri Carboxylic Acid (H3BTC): An Optimization Reaction Condition [C] . W W Lestari, I D Winarni, F Rahmawati Joint Conference on Chemistry . 2017

机译：基于镍（II）和苯1,3,5-三羧酸（H3BTC）的金属 - 有机框架（MOF）的电气结合：优化反应条件
5. Synthesis and characterization of various ruthenium small molecules and metallopolymers for potential use in photovoltaic devices and luminescence properties of N-heterocyclic carbenes and trifluoro methylated tris(pyrazolyl)borate silver (I) acid-base adducts. [D] . Chitikuri, Shylaja. 2012

机译：潜在用于光伏器件的各种钌小分子和金属聚合物的合成和表征，以及N-杂环卡宾和三氟甲基化三（吡唑基）硼酸银（I）酸基加合物的发光性能。
6. Sulfoxide-directed metal-free cross-couplings in the expedient synthesis of benzothiophene-based components of materials [O] . Andrew J. Eberhart, Harry Shrives, Yuntong Zhang, 2016

机译：方便合成材料中苯并噻吩基组分的亚砜定向无金属交叉偶联
7. Retracted Article: An efficient one pot three-component synthesis of 2,4,6-triarylpyridines using triflimide as a metal-free catalyst under solvent-free conditions [O] . Hongshe Wang, Weixing Zhao, Juan Du, 2019

机译：缩回的制品：在无溶剂条件下，在无溶剂条件下，使用三氟乙烯作为金属催化剂的2,4,6-三芳基吡啶的有效三组分合成。
8. Biodegradation Study with 1,3,5-Triazine-2,4-diamine, N2,N2-dimethyl-6- (2,2,2-trifluoro-ethoxy). [R] . 2012

机译：用1,3,5-三嗪-2,4-二胺，N 2，N 2 - 二甲基-6-（2,2,2-三氟 - 乙氧基）进行生物降解研究。

Expedient and efficient one pot synthesis of trifluoroethyl ethers from metal free 2,4,6-tris-(2,2,2-trifluoro-ethoxy)-[1,3,5] triazene

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