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Synthesis of carbon-incorporated titanium oxide nanocrystals by pulsed solution plasma: electrical, optical investigation and nanocrystals analysis

机译：脉冲溶液等离子体合成碳结合的二氧化钛纳米晶体：电学，光学研究和纳米晶体分析

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TiOx/carbon composite nanosheets were synthesized by a "pulsed solution plasma" technique in a Ti-contained solution. The discharge characteristics of the plasma were investigated via the resistance of the plasma channel from current and voltage profiles as a function of capacitor energy. Furthermore, the Ti-based oxides were characterized in detail using high-resolution transmission electron microscopy and selected area electron diffraction. Finally, the formation mechanism of the product was discussed through optical emission spectroscopy. The analyses revealed that the products were composed of spherical nanoparticles of TiO, TiO2 rutile phases and polycrystalline anatase TiO2/carbon composite nanosheets, which were formed by plasma or plasma-induced reactions between species in Ti-contained solution.
机译：通过“脉冲溶液等离子体”技术在含钛溶液中合成了TiOx /碳复合纳米片。通过等离子体通道的电阻，根据电流和电压曲线作为电容器能量的函数，研究了等离子体的放电特性。此外，使用高分辨率透射电子显微镜和选定区域电子衍射对Ti基氧化物进行了详细表征。最后，通过发射光谱研究了产物的形成机理。分析表明，产物由TiO球形纳米颗粒，TiO2金红石相和锐钛矿型TiO2 /碳复合纳米片组成，它们是通过等离子体或等离子体诱导的含钛溶液中物种之间的反应形成的。

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