Two appealing alternatives for MOFs synthesis: solvent-free oven heating vs. microwave heating

Lanchas Monica; Arcediano Sandra; Aguayo Andres T.; Beobide Garikoitz; Castillo Oscar; Cepeda Javier; Vallejo-Sanchez Daniel; Luque Antonio

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Two appealing alternatives for MOFs synthesis: solvent-free oven heating vs. microwave heating

机译：MOF合成的两个有吸引力的替代方法：无溶剂烤箱加热与微波加热

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Herein we present a solvent-free process to afford the synthesis of imidazolate and carboxylate based MOFs performed under moderate oven-heating or fast microwave irradiation, paying special attention to the yield and adsorption performance of the products. The measured adsorption surface area values of the resulting samples compare well, and in several cases surpass, the maximum surface area previously reported for the same compounds prepared using a solvent based synthesis.

机译：本文中，我们提出了一种无溶剂的方法，可以在中等烤箱加热或快速微波辐射下进行咪唑酸酯和羧酸酯基MOF的合成，特别要注意产物的收率和吸附性能。所得样品的测量吸附表面积值进行了很好的比较，在某些情况下甚至超过了以前报道的使用溶剂合成法制备的相同化合物的最大表面积。

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《RSC Advances》 |2014年第104期|共4页
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Lanchas Monica; Arcediano Sandra; Aguayo Andres T.; Beobide Garikoitz; Castillo Oscar; Cepeda Javier; Vallejo-Sanchez Daniel; Luque Antonio;
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中图分类化学;
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1. Two appealing alternatives for MOFs synthesis: solvent-free oven heating vs. microwave heating [J] . Lanchas Monica, Arcediano Sandra, Aguayo Andres T., RSC Advances . 2014,第104期

机译：MOF合成的两个有吸引力的替代方法：无溶剂烤箱加热与微波加热
2. Effects of microwave vs. convection oven heating on the formation of oxidation products in canola (Brassica rapa subsp. oleifera) oil [J] . Jukka-Pekka Suomela, Marko Tarvainen, Heikki Kallio Oilseeds and fats, Crops and Lipids . 2017,第3期

机译：微波对流烤箱加热对低芥酸菜子油中氧化产物形成的影响
3. Microwave-assisted synthesis of various ZnO hierarchical nanostructures: Effects of heating parameters of microwave oven [J] . Zhu PL, Zhang JW, Wu ZS, Crystal growth & design . 2008,第9期

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4. Comparison of Heating Platforms for Fast, High Purity Peptide Synthesis: Infrared Heating on the Tribute~R-IR vs. Microwave Peptide Synthesizers [C] . James P. Cain, Christina A. Chantell, Michael A. Onaiyekan American Peptide Symposium . 2013

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5. Multiphysics modeling to enhance understanding of microwave heating of food in domestic ovens. [D] . Chen, Jiajia. 2015

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6. Comparison of Microwave Short Time and Oven Heating Pretreatment on Crystallization of Raisins [O] . Lorena Alvarez, Paulina Urrutia, Araceli Olivares, 2021

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7. Effects of microwave vs. convection oven heating on the formation of oxidation products in canola (Brassica rapa subsp. oleifera) oil [O] . Jukka-Pekka Suomela, Marko Tarvainen, Heikki Kallio 2017

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Two appealing alternatives for MOFs synthesis: solvent-free oven heating vs. microwave heating

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