Metal-free synthesis of imidazopyridine from nitroalkene and 2-aminopyridine in the presence of a catalytic amount of iodine and aqueous hydrogen peroxide

Tachikawa Yuma; Nagasawa Yoshitomo; Furuhashi Sohei; Cui Lei; Yamaguchi Eiji; Tada Norihiro; Miura Tsuyoshi; Itoh Akichika

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Metal-free synthesis of imidazopyridine from nitroalkene and 2-aminopyridine in the presence of a catalytic amount of iodine and aqueous hydrogen peroxide

机译：在催化量的碘和过氧化氢水溶液存在下，由硝基烯烃和2-氨基吡啶无金属合成咪唑并吡啶

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We have developed a metal-free synthetic method for 3-nitroimidazo[1,2-a] pyridines from nitroalkenes and 2-aminopyridines using catalytic amounts of iodine and aqueous hydrogen peroxide as a terminal oxidant.

机译：我们已经开发了一种无金属的合成方法，该方法使用催化量的碘和过氧化氢水溶液作为末端氧化剂，从硝基烯烃和2-氨基吡啶合成3-硝基咪唑并[1,2-a]吡啶。

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《RSC Advances》 |2015年第13期|共3页
作者
Tachikawa Yuma; Nagasawa Yoshitomo; Furuhashi Sohei; Cui Lei; Yamaguchi Eiji; Tada Norihiro; Miura Tsuyoshi; Itoh Akichika;
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1. Metal-free synthesis of imidazopyridine from nitroalkene and 2-aminopyridine in the presence of a catalytic amount of iodine and aqueous hydrogen peroxide [J] . Tachikawa Yuma, Nagasawa Yoshitomo, Furuhashi Sohei, RSC Advances . 2015,第13期

机译：在催化量的碘和过氧化氢水溶液存在下，由硝基烯烃和2-氨基吡啶无金属合成咪唑并吡啶
2. Samarium mediated pinacol coupling of carbonyl compounds in the presence of a catalytic amount of iodine under aqueous media [J] . Wang Lei, Zhang Yong-Min Chinese Journal of Chemistry . 1999,第5期

机译：在水介质中催化量碘存在下，mar介导的羰基化合物的频哪醇偶联
3. Magnetic nanoparticle-supported imidazole tribromide: a green, mild, recyclable and metal-free catalyst for the oxidation of sulfides to sulfoxides in the presence of aqueous hydrogen peroxide [J] . Otokesh Somayeh, Kolvari Eskandar, Amoozadeh Ali, RSC Advances . 2015,第66期

机译：磁性纳米粒子支持的咪唑三溴化吡唑：在过氧化氢水溶液中，用于氧化硫化硫化物的绿色，温和，可回收和无金属催化剂
4. In situ hydrogen peroxide generation for use as a disinfectant and as an oxidant for water recovery by aqueous phase catalytic oxidation [C] . Akse James R., Atwater James E., Schussel Leonard J., International Conference on Environmental Systems . 1997

机译：原位过氧化氢生成用作消毒剂和作为水相催化氧化水回收的氧化剂
5. Synthesis and characterization of sol-gel-derived xerogel films with antifouling/foul release properties and the preparation, immobilization, and evaluation of a sequestered selenoxide catalyst for brominations with hydrogen peroxide and sodium bromide in an aqueous environment. [D] . Bennett, Stephanie M. 2010

机译：具有防污/防污性能的溶胶-凝胶衍生的干凝胶薄膜的合成和表征，以及在水环境中用于过氧化氢和溴化钠溴化的螯合亚硒酸盐催化剂的制备，固定化和评估。
6. Aqueous Biphasic Systems for the Synthesis of Formates by Catalytic CO2 Hydrogenation: Integrated Reaction and Catalyst Separation for CO2‐Scrubbing Solutions [O] . Martin Scott, Dr. Beatriz Blas Molinos, Christian Westhues, -1

机译：催化CO2加氢合成格式的水两相体系：CO2洗涤溶液的集成反应和催化剂分离
7. Catalytic oxidation of aniline by aqueous hydrogen peroxide in the presence of some heteropolyoxometalates [O] . Mohammad. H. Alizadeh, Reza Tayebee 2005

机译：在一些杂氧酸盐存在下通过过氧化氢水溶液催化氧化苯胺
8. Reactions Involving Hydrogen Peroxide, Iodine, and Iodate Ion. 6. Oxidation of Iodine by Hydrogen Peroxide at 50 deg C. [R] . Liebhafsky, H. A., McGavock, W. C., Reyes, R. J., 1977

机译：涉及过氧化氢，碘和碘酸根离子的反应。 6.过氧化氢在50℃下氧化碘

Metal-free synthesis of imidazopyridine from nitroalkene and 2-aminopyridine in the presence of a catalytic amount of iodine and aqueous hydrogen peroxide

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