Nucleophilic Substitution in 4-Bromo-5-nitrophthalodinitrile: VI.~1 4-Dimethylphenoxy-5-nitrophenoxyphthalodinitrile and the Copper Phthalocyanine Derived from It

V.E.Maizlish; S.A.Ivanovskii; G.P.Shaposhnikov; I.G.Abramov; A.V.Smirnov; V.V.Bakova; N.V.Usoltseva

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Nucleophilic Substitution in 4-Bromo-5-nitrophthalodinitrile: VI.~1 4-Dimethylphenoxy-5-nitrophenoxyphthalodinitrile and the Copper Phthalocyanine Derived from It

机译：4-溴-5-硝基邻苯二甲腈中的亲核取代：VI。〜1 4-二甲基苯氧基-5-硝基苯氧基邻苯二甲腈及其衍生的酞菁铜

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4-(3,4-Dimethylphenoxy)-5-(4-nitrophenoxy)phthalodinitrile was prepared by stepwise nucleophilic substitution of bromine and then the nitro group in 4-bromo-5-nitrophthalodinitrile by the substituted phenoxy groups and was converted to the corresponding octasubstituted copper phthalocyanine by the reaction with copper acetate. The spectroscopic and mesomorphic properties of the resulting complex were studied. It exhibits thermotropic mesomorphism and forms an M phase in the range 85-155 deg C.

机译：溴的逐步亲核取代反应制得4-（3,4-二甲基苯氧基）-5-（4-硝基苯氧基）邻苯二甲腈，然后用取代的苯氧基取代4-溴-5-硝基邻苯二甲腈中的硝基，并转化为相应的由八取代酞菁铜与乙酸铜反应制得。研究了所得配合物的光谱和介晶性质。它表现出热致同质性并在85-155摄氏度范围内形成M相。

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《Russian Journal of General Chemistry》 |2002年第9期|共5页
作者
V.E.Maizlish; S.A.Ivanovskii; G.P.Shaposhnikov; I.G.Abramov; A.V.Smirnov; V.V.Bakova; N.V.Usoltseva;
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1. Nucleophilic Substitution in 4-Bromo-5-nitrophthalodinitrile: VI.~1 4-Dimethylphenoxy-5-nitrophenoxyphthalodinitrile and the Copper Phthalocyanine Derived from It [J] . V.E.Maizlish, S.A.Ivanovskii, G.P.Shaposhnikov, Russian Journal of General Chemistry . 2002,第9期

机译：4-溴-5-硝基邻苯二甲腈中的亲核取代：VI。〜1 4-二甲基苯氧基-5-硝基苯氧基邻苯二甲腈及其衍生的酞菁铜
2. Nucleophilic Substitution in 4-Bromo-5-nitrophthalodinitrile: V.~1 Synthesis of 5-Nitro-4-(4-R-phenoxy) phthalodinitriles and Phthalocyanines Derived from Them [J] . A.V.Balakirev, V.V.Maizlish, G.P.Shaposhnikov Russian Journal of General Chemistry . 2002,第2期

机译：4-溴-5-硝基邻苯二甲腈中的亲核取代：V.〜1合成5-硝基-4-（4-R-苯氧基）邻苯二腈和衍生自它们的酞菁
3. Nucleophilic Substitution of 4-Bromo-5-nitrophthalodinitrile: XVII. Synthesis and Properties of Bifunctionally Substituted Metal Phthalocyanines with Aryloxy and Nitro Groups [J] . Mikhailova A. I., Znoiko S. A., Maizlish V. E., Russian Journal of General Chemistry . 2018,第7期

机译：4-溴-5-硝基硝基二腈的亲核取代：XVII。双甘油氧和硝基双功能取代金属酞菁的合成与性能
4. Corrosion Inhibition of Copper in Chloride Solutions by Different Substituted Copper Phthalocyanines [C] . M. Sancy, M.A. Paez, J.H. Zagal ECS Meeting . 2003

机译：不同取代铜酞菁抗氯化溶液中铜腐蚀抑制作用
5. New Thermally Stable Materials: I. Nucleophilic Azoles with Cyclic Perfluoroalkenes: II. Trifluoromethyl or Pentafluorosulfanyl Substituted Poly-1,2,3-triazoles; and III. Silver and Copper Derivatives of FOX-7 [D] . Garg, Sonali 2010

机译：新的热稳定材料：I.带有环状全氟烯烃的亲核腈：II。用三氟甲基或五氟硫烷基取代的聚1,2,3-三唑;和III。 FOX-7的银和铜衍生物
6. Corrole and nucleophilic aromatic substitution are not incompatible: a novel route to 23-difunctionalized copper corrolates [O] . M. Stefanelli, F. Mandoj, S. Nardis, -1

机译：甲氧基和亲核芳香族取代不是不相容的：23-双官能化铜盐的新途径
7. Erratum to: “Nucleophilic Substitution in 4-Bromo-5-nitrophthalodinitrile: XI. Preparation, Properties, and Prediction of Mesomorphism in Mixed-Substituted Phthalocyanines Containing Aryloxy and Benzotriazole Fragments” [O] . S. A. Znoiko, O. B. Akopova, N. V. Bumbina, 2014

机译：错误：“4-溴-5-硝基丙二腈中的亲核取代：XI。混合取代的含芳氧基和苯并三唑碎片中的混合取代的酞菁中的偏相形的制备，性质和预测“

Nucleophilic Substitution in 4-Bromo-5-nitrophthalodinitrile: VI.~1 4-Dimethylphenoxy-5-nitrophenoxyphthalodinitrile and the Copper Phthalocyanine Derived from It

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