Synthesis and characterization of new stable alpha,omega-organo(bis-silanetriols)

Cerveau G.; Chappellet S.; Corriu RJP.; Dabiens B.; Le Bideau J.

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Synthesis and characterization of new stable alpha,omega-organo(bis-silanetriols)

机译：新型稳定的α，ω-有机（双硅烷三醇）的合成与表征

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Synthesis and characterization of the first stable alpha,omega-bis(silanetriols) containing phenylene, biphenylene, alpha,omega-bis(phenylene)vinylene, alpha,omega-bis(phenylene)ethynylene, and alpha,omega-bis(phenylene)buta-1,3-diynylene organic bridging groups are described. They were obtained by controlled hydrolysis of the corresponding bis(trialkoxysilyl) precursors. An alternative route involving phase-transfer catalysis is also reported. These solids were organized as layers. The triol end groups formed hydrophilic layers, whereas the body of the sheets corresponded to hydrophobic layers. The distance between two neighboring hydrophilic layers was directly related to the length of the organic group; nevertheless, the packing was induced by the hydrogen-bond network. [References: 35]

机译：包含苯，联苯，α，ω-双（亚苯基）亚乙烯基，α，ω-双（亚苯基）乙炔和α，ω-双（亚苯基）丁烯的第一稳定α，ω-双（硅烷三醇）的合成和表征描述了-1，3-二亚炔基有机桥连基团。它们是通过相应双（三烷氧基甲硅烷基）前体的受控水解获得的。还报道了涉及相转移催化的替代途径。这些固体组织为层。三醇端基形成亲水层，而片的主体对应于疏水层。两个相邻的亲水层之间的距离与有机基团的长度直接相关。然而，堆积是由氢键网络引起的。 [参考：35]

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《Organometallics》 |2002年第8期|共5页
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Cerveau G.; Chappellet S.; Corriu RJP.; Dabiens B.; Le Bideau J.;
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中图分类有机化学;有机质材料;
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机译：新型稳定的α，ω-有机（双硅烷三醇）的合成与表征
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Synthesis and characterization of new stable alpha,omega-organo(bis-silanetriols)

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