Synthesis of New 1,3-bis(Heteroaryl)-4,5-imidazolidinediones Through Reaction of N,N'-bis(Heteroaryl)methanediamines with Oxalyl Chloride

Mehdi Ghandi; Farshid Salimi

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Synthesis of New 1,3-bis(Heteroaryl)-4,5-imidazolidinediones Through Reaction of N,N'-bis(Heteroaryl)methanediamines with Oxalyl Chloride

机译：N，N'-双（杂芳基）甲烷二胺与草酰氯反应合成新的1,3-双（杂芳基）-4,5-咪唑烷二酮

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Reaction of N,N'-bis(2-pyridinyl,3-pyridinyl,4-pyridinyl,2-thiazolyl,4-nitrophenyl,and 2-benzothiazolyl)methanediamines 1a-f with oxalyl chloride in dry dichloroethane in the presence of pyridine affords the corresponding 1,3-bis (heteroaryl)-4,5-imidazolidinediones 3a-f in good to excellent yields.The essential role of pyridine in the reaction mixture is described,and reaction details as well as product characterization is discussed.

机译：在吡啶存在下，N，N'-双（2-吡啶基，3-吡啶基，4-吡啶基，2-噻唑基，4-硝基苯基和2-苯并噻唑基）甲烷二胺1a-f与草酰氯在干燥的二氯乙烷中反应制得相应的1,3-双（杂芳基）-4,5-亚咪唑烷二酮3a-f的收率良好至优异。描述了吡啶在反应混合物中的重要作用，并讨论了反应细节和产物表征。

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《Synthetic Communications》 |2007年第6期|共8页
作者
Mehdi Ghandi; Farshid Salimi;
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正文语种 eng
中图分类有机化学;
关键词
4; 5-imidazolidinediones; methanediamine; oxalyl chloride;

机译：4;5-咪唑烷二酮;甲二胺;草酰氯;

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1. Synthesis of New 1,3-bis(Heteroaryl)-4,5-imidazolidinediones Through Reaction of N,N'-bis(Heteroaryl)methanediamines with Oxalyl Chloride [J] . Mehdi Ghandi, Farshid Salimi Synthetic Communications . 2007,第4a6期

机译：N，N'-双（杂芳基）甲烷二胺与草酰氯反应合成新的1,3-双（杂芳基）-4,5-咪唑烷二酮
2. Synthesis of 1-heteroaryl-and 1,3-bis(heteroaryl)azulenes: Electrophilic heteroarylation of azulenes with the triflates of N-containing heteroarenes [J] . Shoji T., Ito S., Higashi J., European journal of organic chemistry . 2011,第27期

机译：1-杂芳基和1,3-双（杂芳基）氮杂唑的合成：天青石与含氮杂芳基三氟甲磺酸酯的亲电杂芳基化
3. Synthesis of 5-Heteroaryl- and 5,7-Bis(heteroaryl)azulenes by Electrophilic Substitution of 1,3-Di-tert-Butylazulene with Triflates of N-Containing Heterocycles [J] . Shoji T, Ito S, Toyota K, European journal of organic chemistry . 2010,第6期

机译：1,3-二叔丁基az杂腈与N-杂环三氟甲酸酯的亲电取代反应合成5-杂芳基和5,7-双（杂芳基））
4. Rhodium-catalyzed Synthesis of Unsymmetric Di(heteroaryl) Compounds Using Heteroaryl Exchange Reactions [C] . Mieko Arisawa 日本化学会春季年会講演予稿集 . 2018

机译：使用杂芳基交换反应的铑催化的非对称二（杂芳基）化合物的合成
5. Functionalized organotrifluoroborates: Synthesis and reactivity. I.Suzuki-Miyaura reactions of aryl- and heteroaryl trifluoroborates with aryl- and heteroaryl triflates. II. Oxidation of hydroxyl-containing trifluoroborates. III. Suzuki-Miyaura reactions of potassium trifluoroboratohomoenolates. IV. Development of a HRMS method for organotrifluoroborates [D] . Petrillo, Daniel E. 2008

机译：功能化的有机三氟硼酸酯：合成与反应性。芳基-和杂芳基三氟硼酸酯与芳基-和杂芳基三氟甲磺酸酯的I.Suzuki-Miyaura反应。二。含羟基的三氟硼酸盐的氧化。三，三氟硼硼酸同戊烯酸钾的Suzuki-Miyaura反应。 IV。研发有机三氟硼酸盐的HRMS方法
6. Addition of Organochromium Reagents to Heteroaryl Aldehydes. Synthesis of Heteroaryl Substituted bis-Allyl Ethers and Homoallyl Ethers [O] . S. Servi, C. Topaloglu 2004

机译：在杂芳基醛中添加有机铬试剂。杂芳基取代的双烯丙基醚和均烯丙基醚的合成
7. Amberlite IRA-400 Cl resin catalyzed synthesis of secondary amines and transformation into N-((1H-indol-3-yl) (heteroaryl) methyl)-N-heteroaryl benzenamines and bis-indoles via multicomponent reaction [O] . Harichandran Gurusamy, David Amalraj Savarimuthu, Shanmugam Ponnusamy 2016

机译：Amberlite IRA-400 Cl树脂催化仲胺的合成并通过多组分反应转化为N-（（（1H-吲哚-3-基）（杂芳基）甲基）-N-杂芳基苯并胺和双吲哚

Synthesis of New 1,3-bis(Heteroaryl)-4,5-imidazolidinediones Through Reaction of N,N'-bis(Heteroaryl)methanediamines with Oxalyl Chloride

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