Selective reductions of C-(4,6-O-benzylidene-beta-D-glucopyranosyl) nitromethane

Simo O; Michael K; Yoshida W; Chertkov VA; Gross PH

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Selective reductions of C-(4,6-O-benzylidene-beta-D-glucopyranosyl) nitromethane

机译：C-（4,6-O-亚苄基-β-D-吡喃葡萄糖基）硝基甲烷的选择性还原

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摘要

The nitromethyl group of C-(4,6-O-benzylidene-beta-D-glucopyranosyl) nitromethane was manipulated by various reduction and oxidation methods and further functionalizations into -CH2NHOH, -CH=NOH, -CN, -CH=O, and -CH2NHCONH2, all with retention of the 4,6-O-benzylidene group. Certain reduction methods gave rise to a novel secondary amine via an unusual dimeric aminal.

机译：通过各种还原和氧化方法处理C-（4,6-O-亚苄基-β-D-吡喃葡萄糖基）硝基甲烷的硝基甲基基团，并将其进一步官能化为-CH2NHOH，-CH = NOH，-CN，-CH = O，和-CH 2 NHCONH 2，均保留了4，6-O-亚苄基。某些还原方法通过不寻常的二聚缩醛胺产生了新型仲胺。

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《Synthetic Communications》 |2005年第12期|共11页
作者
Simo O; Michael K; Yoshida W; Chertkov VA; Gross PH;
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正文语种 eng
中图分类有机化学;
关键词
C-glycosides; dimerization; nitro methyl; protective groups; reduction; C-GLYCOSIDE SYNTHESES; HENRY CONDENSATIONS; D-GLUCOSE; ROUTE; ACIDS;

机译：C-糖苷;二聚;硝基甲基;保护基;还原;C-糖苷合成;亨利缩合;D-葡萄糖;路线;酸;

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机译：C-（4,6-O-亚苄基-β-D-吡喃葡萄糖基）硝基甲烷的选择性还原
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机译：氧化还原催化与底物光氧化反应的催化剂再生通过底物还原。 W10O324催化的硫醚同时氧化C-H键断裂和还原C-s键断裂

Selective reductions of C-(4,6-O-benzylidene-beta-D-glucopyranosyl) nitromethane

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