An efficient method for the synthesis of acylals from aldehydes under solvent-free conditions catalyzed by antimony trichloride

Bhattacharya AK; Mujahid M; Natu AA

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An efficient method for the synthesis of acylals from aldehydes under solvent-free conditions catalyzed by antimony trichloride

机译：三氯化锑催化无溶剂条件下由醛合成酰基的有效方法

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摘要

A mild and efficient method has been developed for the preparation of acylals from aldehydes catalyzed by antimony trichloride under solvent-free conditions in very good to excellent yields. The easy availability, low cost, and ease of handling of the catalyst make this procedure especially attractive for large-scale synthesis.

机译：已开发出一种温和而有效的方法，可在无溶剂条件下，由三氯化锑催化的醛类制备酰基化合物，收率非常好。容易获得，低成本和易于处理的催化剂使得该方法对于大规模合成特别有吸引力。

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《Synthetic Communications》 |2008年第3期|共7页
作者
Bhattacharya AK; Mujahid M; Natu AA;
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正文语种 eng
中图分类有机化学;
关键词
acetic anhydride; acylals; aldehydes; antimony trichloride; solvent-free conditions;

机译：乙酸酐;酰基醛;醛;三氯化锑;无溶剂条件;

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专利

1. An Efficient Method for the Synthesis of Acylals from Aldehydes under Solvent-Free Conditions Catalyzed by Antimony Trichloride [J] . Synthetic Communications . 2008,第1期

机译：三氯化锑无溶剂条件下由醛类合成醛的有效方法
2. An efficient method for the synthesis of acylals from aldehydes under solvent-free conditions catalyzed by antimony trichloride [J] . Bhattacharya AK, Mujahid M, Natu AA Synthetic Communications . 2008,第1a3期

机译：三氯化锑催化无溶剂条件下由醛合成酰基的有效方法
3. A Mild and Efficient Method for the Synthesis of Acylals from Aromatic Aldehydes and Their Deprotections Catalyzed by Synthetic Phosphates under Solvent-Free Conditions [J] . Fathallaah Bazi, Bahija Mounir, Mohammed Hamza, Green and Sustainable Chemistry . 2018,第4期

机译：一种无溶剂条件下由芳香醛合成酰基的轻度高效方法及合成磷酸盐的脱保护
4. Synthesis of bis-indolylmethanes containing 1,2,3-triazolyl catalyzed by Bransted acidic ionic liquid under solvent-free conditions [C] . Yonghong Zhang, Zhenkai Lei, Xiangju Huang International Conference on Advanced Engineering Materials and Technology . 2011

机译：在无溶剂条件下合成含有Bransted酸性离子液体催化的1,2,3-三唑基的双吲哚甲基甲烷
5. Part I. Asymmetric organocatalysis: (1) Direct enantioselective organocatalytic hydroxymethylation of aldehydes catalyzed by alpha,alpha-diphenylprolinol trimethylsilyl ether: Application in the formal synthesis of (-)-Rasfonin; (2) Synthesis of a novel bicyclic secondary amine organocatalyst: Application to the direct enantioselective organocatalytic hydroxymethylation of aldehydes. Part II. Asymmetric synthesis of bicyclic analogues of the anti-osteoporotic drug risedronate. [D] . Miller, John Robert. 2010

机译：第一部分，不对称有机催化：（1）α，α-二苯基脯氨醇三甲基甲硅烷基醚催化的醛的直接对映选择性有机催化羟甲基化：在（-）-Rasfonin的正式合成中的应用；（2）新型双环仲胺有机催化剂的合成：应用于醛的直接对映选择性有机催化羟甲基化。第二部分抗骨质疏松药物Risedronate的双环类似物的不对称合成。
6. NaHSO4-SiO2 as an efficient and chemoselective catalyst for the synthesis of acylal from aldehydes under solvent-free conditions [O] . Ravi Kumar Kannasani, V V Satyanarayana Peruri, Srinivasa Reddy Battula 2012

机译：NaHSO4-SiO2是一种高效的化学选择性催化剂可在无溶剂条件下从醛类合成酰基
7. NaHSO₄-SiO₂ as an efficient and chemoselective catalyst, for the synthesis of acylal from aldehydes under, solvent-free conditions [O] . Kannasani Ravi Kumar, Peruri V V Satyanarayana, Battula Srinivasa Reddy 2012

机译：NaHSO _{4 -SiO _{2 是一种高效的化学选择性催化剂，可在无溶剂条件下从醛类合成酰基}}

An efficient method for the synthesis of acylals from aldehydes under solvent-free conditions catalyzed by antimony trichloride

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