Kresoxim-Methyl: A Method of Residue Analysis by HPLC

RS Hosmani; SP Nayak; Savita Prithviraj

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Kresoxim-Methyl: A Method of Residue Analysis by HPLC

机译：Kresoxim-Methyl：HPLC残留分析方法

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A simple H PLC method for the analysis of residues of kresoxim-methyl in food commodities ie grape, paddy grain and paddy straw, soil and water. The method involved extraction of the samples using acetone, clean-up by liquid-liquid partitioning with dichloromethane followed by adsorption column chromatography using silica gel as adsorbent and the final estimation by high performance liquid chromatography (HPLC) with UV detector. The method gave good recoveries ranging between 70-100%, with no interference from matrix co-extractives and with achievable limit of determination as 0.02 μg g~(-1).

机译：一种简单的H PLC方法，用于分析食品中葡萄，稻谷和稻草，土壤和水的残留量。该方法包括使用丙酮萃取样品，通过二氯甲烷进行液-液分配进行净化，然后使用硅胶作为吸附剂的吸附柱色谱法以及通过带有UV检测器的高效液相色谱法（HPLC）进行最终估算。该方法回收率在70-100％之间，不受基质共萃取物的干扰，测定极限为0.02μgg〜（-1）。

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《Pesticide Research Journal》 |2008年第2期|共5页
作者
RS Hosmani; SP Nayak; Savita Prithviraj;
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正文语种 eng
中图分类化学工业;
关键词
HPLC-UV; kresoxim-methyl; strobilurin fungicides; residue analysis;

机译：HPLC-UV;kresoxim-methyl;strobilurin杀菌剂;残留分析;

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专利

1. Kresoxim-Methyl: A Method of Residue Analysis by HPLC [J] . RS Hosmani, SP Nayak, Savita Prithviraj Pesticide Research Journal . 2008,第2期

机译：Kresoxim-Methyl：HPLC残留分析方法
2. Orthogonal optimization of extraction and analysis for red wine residues in simulated and archaeological materials using LC/MS and HPLC methods [J] . Zhang Tianxi, Xu Shanhui, Li Yinli, Microchemical Journal: Devoted to the Application of Microtechniques in all Branches of Science . 2018,第期

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3. Analysis of residue dynamics of clofentezine in tangerine and field soil by QuEChERS and HPLC-UV methods [J] . Hai Hong, Yuanyuan Yang, Qiliang Huang, International journal of environmental analytical chemistry . 2014,第6a10期

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4. Multi-residue Antibiotic Analysis of Dairy Products using UHPLC-MS/MS with a Heated Laminar Flow Interface and a Modified QuEChERS Method [C] . A. Dalmia, T. White, S. Reddy, ASMS Conference on Mass Spectrometry and Allied Topics . 2016

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6. Dissipation Dynamics and Dietary Risk Assessment of Kresoxim-Methyl Residue in Rice [O] . MingNa Sun, Lu Yu, Zhou Tong, 2019

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Kresoxim-Methyl: A Method of Residue Analysis by HPLC

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