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首页> 外文期刊>Philosophical Magazine Letters >Transmission electron microscopy-energy-dispersive X-ray spectroscopy analysis of the modulated structure in ZrO_2-6 mol% Y_2O_3 alloy
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Transmission electron microscopy-energy-dispersive X-ray spectroscopy analysis of the modulated structure in ZrO_2-6 mol% Y_2O_3 alloy

机译:ZrO_2-6 mol%Y_2O_3合金调制结构的透射电子显微镜-能量色散X射线光谱分析

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摘要

The modulated structure formed in ZrO_2-6 mol% Y_2O_3 alloy annealed at 1200 ℃ for 126 h has been analysed by nanoprobe analytical electron microscopy. Transmission electron microscopy-energy-dispersive X-ray spectroscopy analysis revealed that the Y-to-Zr ratio fluctuates along a direction perpendicular to the dark and bright lamellae of the modulated structure. The fluctuation arises in a composition range between 1 and 8 mol% Y_2O_3 with a wavelength of about 15 nm. The dark and bright contrast is shown to be associated with the compositional fluctuation, which must be formed by spinodal decomposition.
机译:通过纳米探针分析电子显微镜分析了在1200℃退火126h的ZrO_2-6mol%Y_2O_3合金中形成的调制结构。透射电子显微镜-能量色散X射线光谱分析表明,Y与Zr之比沿垂直于调制结构的暗和亮薄片的方向波动。在约15nm的波长下,在1至8mol%的Y_2O_3的组成范围内出现波动。暗和亮的对比度显示出与成分波动有关,成分波动必须通过旋节线分解形成。

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