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Hot isostatic pressing of bulk magnesium diboride: mechanical and superconducting properties

机译:块状二硼化镁的热等静压:机械和超导性能

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Hot isostatic pressing with glass encapsulation (pressure, 200MPa; temperature, 1000 ℃ over 200 min; cooling under pressure) was used to synthesize bulk MgB_2 with diameters up to 20 mm and thicknesses up to 10 mm from MgB_2 powder. A sharp superconducting transition was measured at 38.5 K. This method can be scaled to larger sample sizes and complex shapes. The data for density, microhardness, fracture toughness and sound speed for bulk magnesium diboride are presented. Ball milling the powder results in a more homogeneous final microstructure with a higher resistivity and with a similar superconducting transitions.
机译:采用玻璃封装的热等静压工艺(压力200MPa;温度1000℃,历时200min;加压冷却),由MgB_2粉末合成直径最大为20mm,厚度最大为10mm的块状MgB_2。在38.5 K处测量到一个尖锐的超导跃迁。该方法可以扩展到更大的样本大小和复杂的形状。给出了块状二硼化镁的密度,显微硬度,断裂韧性和声速数据。将粉末进行球磨可得到具有更高电阻率和类似超导转变的更均匀的最终微观结构。

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