首页> 外文期刊>Studia Universitatis Babes-Bolyai. Series Physica >INFLUENCE OF THE SINTERING TEMPERATURE ONSTRUCTURE, ELECTRIC AND MECHANICALPROPERTIES OF THE POLYCRYSTALLINE(Bi,Pb):2223 SUPERCONDUCTORS
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INFLUENCE OF THE SINTERING TEMPERATURE ONSTRUCTURE, ELECTRIC AND MECHANICALPROPERTIES OF THE POLYCRYSTALLINE(Bi,Pb):2223 SUPERCONDUCTORS

机译:烧结温度(Bi,Pb):2223超导体的温度结构,电学和力学性能的影响

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摘要

Bulk superconducting materials with nominal composition(Bi_(1.6)Pb_(0.4))(Sr_(1,8)Ba_(0,2))Ca_2Cu_3O_ywere synthesized by solid state reaction method byusing different sintering temperature ( in the range 840°C- 850°C). X-raydiffraction pattern shows that in all samples the majority phase is 2223, with sometraces of Bi:2212. The electrical properties of the samples were examined byelectrical resistance versus temperature, R(T). By using the linear behavior forR(T), the influence of sintering temperature on the parameters related to inter-grainresistivity and the percolation conduction were evaluated. To study the mechanicalproperties of Bi:2223 samples, Vickers micro hardness were measured. The variationof micro hardness with load is nonlinear, and described by Mayer's law.
机译:使用不同的烧结温度(在840°C-850范围内)通过固态反应方法合成了标称组成为(Bi_(1.6)Pb_(0.4))(Sr_(1,8)Ba_(0,2))Ca_2Cu_3O_y的块状超导材料°C)。 X射线衍射图表明,在所有样品中,主要相为2223,具有一些痕量的Bi:2212。通过电阻对温度R(T)检验样品的电性能。通过使用R(T)的线性行为,评估了烧结温度对与晶间电阻率和渗流传导相关的参数的影响。为了研究Bi:2223样品的力学性能,测量了维氏显微硬度。显微硬度随载荷的变化是非线性的,并由迈耶定律描述。

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