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Component extraction and separation apparatus using supercritical fluid and component extraction and separation method

机译:使用超临界流体的成分提取分离装置及成分提取分离方法

摘要

PROBLEM TO BE SOLVED: To provide a component extracting and separating device and a component extracting and separating method, both using supercritical fluid, that make available spectra reduced in baseline fluctuations attributable to pressure fluctuations.SOLUTION: A component extracting and separating device comprises a channel 111 that passes a mobile phase and a sample to a column 11; a regulator 14 that adjusts pressure applied on the mobile phase in the channel 111 to a pressure surpassing a critical pressure, which turns the mobile phase in the column 11 into a supercritical state; a column oven 12 for heating the column 11 to a temperature surpassing a critical temperature; a cooler 130 that cools the mobile phase having passed the column 11; and a detector 13 that detects components of the sample in the mobile phase cooled by the cooler 130.
机译:解决的问题:提供一种均使用超临界流体的成分提取和分离装置以及成分提取和分离方法,以使可归因于压力波动的基线波动减少的光谱可用。 111使流动相和样品通过色谱柱11;调节器14将施加在通道111中的流动相的压力调节到超过临界压力的压力,该压力使塔11中的流动相变成超临界状态。柱炉12,用于将柱11加热到超过临界温度的温度;冷却器130冷却通过塔11的流动相。检测器13检测由冷却器130冷却后的流动相中的样品成分。

著录项

  • 公开/公告号JP6269345B2

    专利类型

  • 公开/公告日2018-01-31

    原文格式PDF

  • 申请/专利权人 株式会社島津製作所;

    申请/专利号JP20140130383

  • 发明设计人 舟田 康裕;

    申请日2014-06-25

  • 分类号G01N30/02;G01N30/54;G01N30/30;G01N30/84;

  • 国家 JP

  • 入库时间 2022-08-21 13:07:35

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