首页> 外国专利> Apparatus and Method for Absorption, Emission, and Scattering Spectroscoy With Substantially Simultaneous Mass Spectrometry, and Apparatus and Method for Mass Spectrometry Based on Electrospray Ionization

Apparatus and Method for Absorption, Emission, and Scattering Spectroscoy With Substantially Simultaneous Mass Spectrometry, and Apparatus and Method for Mass Spectrometry Based on Electrospray Ionization

机译:基本上同时进行质谱分析的吸收光谱,发射光谱和散射光谱的仪器和方法,以及基于电喷雾电离的质谱分析仪器和方法

摘要

An ionization chamber of an analytical apparatus (10) in which high concentration test sample ions are evaporated is provided with an ion introduction control means (8) to control the quantity of the test sample ions introduced to an ion attracting electrode (9). Therefore, an analytical apparatus can be provided that is capable of substantially simultaneous mass spectrometry and absorption, emission, and scattering spectroscopy. The apparatus also includes: a low temperature bath (106) which cools the test sample solution before it is introduced to the sprayer (104); and a cooling gas introduction tube (108), constructed separately from the sprayer, which cools the sprayer and the test sample solution introduced to the sprayer (104). The inclusion enables effective restriction of test sample heating upon high voltage application. Mass spectrometry and absorption, emission, and scattering spectroscopy can be substantially simultaneously carried out even when the test sample used is stable only at extremely low temperatures.
机译:在蒸发了高浓度测试样品离子的分析设备( 10 )的电离室中,设有离子导入控制装置( 8 )以控制离子注入量。测试样品离子被引入离子吸引电极( 9 )。因此,可以提供一种能够基本上同时进行质谱分析和吸收,发射和散射光谱分析的分析设备。该设备还包括:低温浴( 106 ),其在将测试样品溶液引入喷雾器之前对其进行冷却( 104 );与喷雾器分开构造的冷却气体引入管( 108 ),用于冷却喷雾器和引入喷雾器的测试样品溶液( 104 )。内含物可有效限制施加高压后测试样品的加热。即使所使用的测试样品仅在极低的温度下才是稳定的,质谱分析,吸收,发射和散射光谱分析也可以同时进行。

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