Suzuki-Miyaura Reaction, Novel Synthesis of C-N and N-N Ligands for Organic Light-Emitting Devices

机译：Suzuki-Miyaura反应，新颖的C-N和N-N配体用于有机发光器件

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The Pd(II)-catalyzed cross-coupling Suzuki-Miyaura reaction of aryl boronic acid and aryl halide was investigated. We found that 1% PdCl_2(PPh_3)_2, 10% PPh_3 and 1 M Na_2CO_3 (aq.) in refluxing 1,4-dioxane for 4 hours is the optimize condition. The desired products e.g. 2-phenyl pyridine and bipyridine derivatives were obtained in moderate to excellent yields.

机译：研究了Pd（ii） - 催化芳基硼酸和芳基卤化物的交叉偶联Suzuki-miyaura反应。我们发现在回流1,4-二恶烷4小时时，1％PdCl_2（PPH_3）_2,10％PPH_3和1M NA_2CO_3（AQ）是优化条件。所需产品例如将2-苯基吡啶和双吡啶衍生物中等至优异的产率获得。

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《International Conference on Manufacturing Science and Technology》|2013年||共5页
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作者
Namthip Khammultri; Nichapha Senamart; Nunthiya Deepuppha; Kittiya Wongkhan; Rukkiat Jitchati;
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中图分类 TH16-53;
关键词
Suzuki-Miyaura reaction; Ligand synthesis; OLED; Triphenylphosphine;

机译：铃木宫达反应;配体合成;OLED;三苯基膦;

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1. Synthesis, characterization, electrochemical behaviors and applications in the Suzuki-Miyaura cross-coupling reactions of N_2S_2O_2 thio Schiff base ligand and its Cu(II), Co(III), Ni(II), Pd(II) complexes and their usage in the fabrication of organic-inorganic hybrid devices [J] . Hamdi Temel, Salih Pasa, Yusuf Selim Ocak Synthetic Metals . 2011,第23a24期

机译：N_2S_2O_2硫代席夫碱配体及其Cu（II），Co（III），Ni（II），Pd（II）配合物的Suzuki-Miyaura偶联反应的合成，表征，电化学行为及其应用有机-无机混合器件的制造
2. Recent Applications of Aryltriazenes in Organic Synthesis via C-N/N-N Bond Cleavage [J] . Zhang Yonghong, Cao Dawei, Liu Wenbo, Current organic chemistry . 2015,第2期

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3. Mixed-ligand benzaldehyde thiosemicarbazone complexes of palladium containing triphenylphosphine as ancillary ligand : Synthesis, structure and catalytic application in C-N coupling reactions [J] . Jayita Dutta, Samaresh Bhattacharya Journal of the Indian Chemical Society . 2014,第4期

机译：含三苯基膦作为辅助配体的钯的混合配体苯甲醛硫半脲配合物：C-N偶联反应的合成，结构及催化应用
4. Suzuki-Miyaura Reaction, Novel Synthesis of C-N and N-N Ligands for Organic Light-Emitting Devices [C] . Namthip Khammultri, Nichapha Senamart, Nunthiya Deepuppha, International Conference on Manufacturing Science and Technology . 2013

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Suzuki-Miyaura Reaction, Novel Synthesis of C-N and N-N Ligands for Organic Light-Emitting Devices

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