Isoquinoline-catalyzed reaction between 4-hydroxycoumarin or 4-hydroxy-6-methylpyran-1-one and dialkyl acetylene dicarboxylates: synthesis of coumarin and pyranopyrane derivatives

Hamid Reza Khavasi; Hossein Anaraki-ardakani; Mohammad Anary-abbasinejad; Mohammad Hossein Mosslemin

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Isoquinoline-catalyzed reaction between 4-hydroxycoumarin or 4-hydroxy-6-methylpyran-1-one and dialkyl acetylene dicarboxylates: synthesis of coumarin and pyranopyrane derivatives

机译：异喹啉催化4-羟基香豆素或4-羟基-6-甲基吡喃-1-酮与乙炔二羧酸二烷基酯的合成：香豆素和吡喃并吡喃衍生物的合成

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In this work we report the reaction between dialkyl acetylenedicarboxylates and enolic systems such as 5,5-dimethyl-1,3-cyclohexanedione, 1,3-cyclohexanedione, 4-hydroxycoumarin or 4-hydroxy-6-methylpyran-1-one in the presence of isoquinoline, which leads to new coumarin and pyranopyran derivatives.

机译：在这项工作中，我们报告了乙炔二羧酸二烷基酯与烯醇体系（如5,5-二甲基-1,3-环己二酮，1,3-环己二酮，4-羟基香豆素或4-羟基-6-甲基吡喃-1-酮）之间的反应。异喹啉的存在，会导致新的香豆素和吡喃并吡喃衍生物。

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《Journal of the Brazilian Chemical Society》 |2010年第2期|共5页
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Hamid Reza Khavasi; Hossein Anaraki-ardakani; Mohammad Anary-abbasinejad; Mohammad Hossein Mosslemin;
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中图分类生物物理学;
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1. Isoquinoline-Catalyzed Reaction between 4-Hydroxycoumarin or4-Hydroxy-6-methylpyran-l-one and Dialkyl Acetylene Dicarboxylates:Synthesis of Coumarin and Pyranopyrane Derivatives [J] . Mohammad Anary-Abbasinejad, Hossein Anaraki-Ardakani, Mohammad Hossein Mosslemin, Journal of the Brazilian Chemical Society . 2010,第2期

机译：异喹啉催化4-羟基香豆素或4-羟基-6-甲基吡喃-1-酮与乙炔基二羧酸二烷基酯的反应：香豆素和吡喃并吡喃衍生物的合成
2. One-pot, three-component synthesis of dialkyl 1,2-dihydroquinoline-2,3-dicarboxylates from triphenylphosphine, acetylenic esters, and amide derivatives of 2-aminobenzaldehyde in aqueous acetone [J] . Ramazani A, Ahmadi E, Kazemizadeh AR, Phosphorus, Sulfur, and Silicon and the Related Elements . 2005,第11期

机译：由三苯基膦，炔属酯和2-氨基苯甲醛的酰胺衍生物在丙酮水溶液中一锅三组分合成1,2-二氢喹啉-2,3-二羧酸二烷基酯
3. Synthesis of unexpected novel bis-coumarin derivatives via three component reactions of 4-hydroxycoumarin, aldehydes and cyclic secondary amines. Conformation in the solid state and pharmacological evaluation [J] . Fatma A.El-Samahy, Hayam A. AbdEl Salam, Naglaa F.El-Sayed, Zeitschrift fur Naturforschung, B. A Journal of Chemical Sciences . 2017,第10期

机译：通过4-羟基苏林，醛和环仲胺的三种组分反应合成意外的新型BIS-COUMARIN衍生物。坚实状态和药理学评估
4. The Synthesis and Characterization of Nadic Dialkyl-Ester Derivatives with Trialkyl Borate [C] . JIN YIWEN, Jun Seong Park, Yong Sung Park, International Conference on Advances in Materials and Manufacturing Processes . 2012

机译：用三烷基硼酸盐的纳米二烷基酯衍生物的合成与表征
5. Green chemistry in pyrrole synthesis. I. Solvent effect in Barton-Zard pyrrole synthesis: An improved synthesis of 3,4-dialkyl-1H-pyrrole-2-carboxylates. II. A novel route for the synthesis of pharmaceutically important pyrrole derivatives. [D] . Cherukuri, Sankara R. 2005

机译：吡咯合成中的绿色化学。 I.Barton-Zard吡咯合成中的溶剂作用：3，4-二烷基-1H-吡咯-2-羧酸酯的改进的合成。二。合成重要的吡咯衍生物的新途径。
6. Benzylidene-bis-(4-Hydroxycoumarin) and Benzopyrano-Coumarin Derivatives: Synthesis 1H/13C-NMR Conformational and X-ray Crystal Structure Studies and In Vitro Antiviral Activity Evaluations [O] . Davorka Završnik, Samija Muratović, Damjan Makuc, 2011

机译：亚苄基双（4-羟基香豆素）和苯并吡喃-香豆素衍生物：合成1H / 13C-NMR构象和X射线晶体结构研究和体外抗病毒活性评估
7. Isoquinoline-catalyzed reaction between 4-hydroxycoumarin or 4-hydroxy-6-methylpyran-1-one and dialkyl acetylene dicarboxylates: synthesis of coumarin and pyranopyrane derivatives [O] . Mohammad Anary-Abbasinejad, Hossein Anaraki-Ardakani, Mohammad Hossein Mosslemin, 2010

机译：异喹啉催化剂催化4-羟基苏林或4-羟基-6-甲基吡喃-1-α和二烷基乙炔二羧酸盐：合成香豆素和吡喃芘衍生物
8. Phase Transfer Pd(O) Catalyzed Polymerization Reactions. 1. Synthesis of 1,2-(4,4'-Dialkoxyaryl)Acetylene Monomers and 1,4-Bis(2-(4',4''-Dialkoxyphenyl)Ethynyl)Benzene Derivatives by Phase Transfer Pd(O)/Cu(I) Catalyzed Coupling Reactions. [R] . Pugh, C., Percec, V. 1990

机译：相转移pd（O）催化的聚合反应。 1.相转移pd（O）/ Cu合成1,2-（4,4'-二烷氧基芳基）乙炔单体和1,4-双（2-（4'，4'-二烷氧基苯基）乙炔基）苯衍生物（I）催化的偶联反应。

Isoquinoline-catalyzed reaction between 4-hydroxycoumarin or 4-hydroxy-6-methylpyran-1-one and dialkyl acetylene dicarboxylates: synthesis of coumarin and pyranopyrane derivatives

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