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Three years monitoring survey of pesticide residues in Sardinia wines following integrated pest management strategies

机译:结合病虫害综合防治策略对撒丁岛葡萄酒中的农药残留进行三年监测

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摘要

This paper reports the results of a pesticide monitoring survey on wine grapes from the 2008— 2010 vintage from vineyards grown according to integrated pest management strategies. A multi-residue gas chromatography-mass spectrometry method in electron ionization and chemical ionization mode has been used for the determination of 30 pesticides in wine samples. The analytical method showed good recoveries and allowed a good separation of the selected pesticides. Repeatability and intermediate precision showed good results with CV<20 %. The instrumental method limits of determination (LOD) and of quantification (LOQ) were below the maximum residue levels set in wine. The analysis of the wines showed that pesticide residues were below the instrumental LOQ, and most of them were unde-tectable (
机译:本文报告了一项农药监测调查的结果,该监测结果是根据有害生物综合治理策略,从2008-2010年份的葡萄园收获的酿酒葡萄。采用电子电离和化学电离模式的多残留气相色谱-质谱法测定葡萄酒样品中的30种农药。该分析方法显示出良好的回收率,并能很好地分离出所选农药。 CV <20%时,重复性和中间精度显示出良好的结果。仪器方法的测定极限(LOD)和定量极限(LOQ)低于葡萄酒中设定的最大残留水平。对葡萄酒的分析表明,农药残留低于仪器的最低定量限,而且大多数残留物不可检测(

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  • 来源
    《Environmental Monitoring and Assessment》 |2013年第5期|4281-4289|共9页
  • 作者单位

    Department of Life Science and Environment,University of Cagliari,via Ospedale 72,09124 Cagliari, Italy;

    Agricultural Research Agency of Sardinia (AGR1S),07100, Bonassai SS 291 km 18,6,Sassari, Italy;

  • 收录信息 美国《科学引文索引》(SCI);美国《工程索引》(EI);美国《化学文摘》(CA);
  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类
  • 关键词

    pesticide residues; wine; ipm; gc-itms;

    机译:农药残留;葡萄酒;ipm;gc-itms;

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