首页> 外文期刊>International journal of nanomechanics science and technology >SYNTHESIZATION, ELECTRICAL AND THERMAL PROPERTIES OF Ni-SUBSTITUTED NANOFERRITE PARTICLES
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SYNTHESIZATION, ELECTRICAL AND THERMAL PROPERTIES OF Ni-SUBSTITUTED NANOFERRITE PARTICLES

机译:镍取代的纳米铁矿颗粒的合成,电学和热学性质

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摘要

Nanoferrite particles were synthesized by a coprecipitation method with the composition of x = 0.00, x = 0.10, x = 0.20, x = 0.40. The powder samples were characterized by X-ray diffraction (XRD), scanning electron microscope (SEM), two-point probe method, and thermogravimetric analysis-differential temperature analysis (TG-DTA). The average crystallite sizes of particles were determined from XRD. The X-ray analysis showed that the samples were cubic spinel. The average crystallite size (D_(ave)) of the particles precipitated was found to vary from 14.25 nm to 9.50 nm, decreasing with increase in nickel substitution. The results of the present study reveal that nanoferrites have higher resistivity, are thermally stable, and there is an improvement in the stability due to the dopants added to compounds. The present results point to the possibility of using the investigated samples for high frequency applications and electronic applications.
机译:通过共沉淀法合成具有x = 0.00,x = 0.10,x = 0.20,x = 0.40的组成的纳米铁氧体颗粒。通过X射线衍射(XRD),扫描电子显微镜(SEM),两点探针法和热重分析-差温分析(TG-DTA)对粉末样品进行表征。从XRD确定颗粒的平均微晶尺寸。 X射线分析表明样品为立方尖晶石。发现沉淀的颗粒的平均微晶尺寸(D_(ave))在14.25nm至9.50nm之间变化,随着镍取代的增加而减小。本研究的结果表明,纳米铁氧体具有较高的电阻率,具有热稳定性,并且由于向化合物中添加了掺杂剂,因此稳定性得到了改善。目前的结果指出了将所研究的样品用于高频应用和电子应用的可能性。

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