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Formation of Single-Walled Carbon Nanotube Buckybooks, Graphene Nanosheets and Metal Decorated Graphene

机译:单壁碳纳米管Buckybooks,石墨烯纳米片和金属装饰石墨烯的形成

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摘要

The various carbon nanostructures e.g. single-walled carbon nanotubes (SWCNTs) web, graphene nanosheets and metal nanoparticle decorated graphene sheets have been synthesized in large quantity by electrical arc discharge method under an argon atmosphere. The as-synthesized nanostructures were characterized by different characterization techniques such as XRD, SEM, TEM, Energy dispersive X-ray spectroscopy, Raman and FTIR spectroscopy. The SWCNT webs of length ~6 cm abundantly containing aligned SWCNTs have diameter of about 1.8 nm and form buckybook like structure. Few layer graphene (FLG) sheets were prepared by electric arc discharge of high purity graphite electrodes in a varying argon gas atmosphere (250-500T). The largest areal extent of graphene (with lowest number of layer i.e. four) has been found at 350T argon pressure. A one step method is also reported for the decoration of these graphene nanosheets with iron and nickel nanoparticles through arc discharge method.
机译:各种碳纳米结构例如单壁碳纳米管(SWCNTs)幅材,石墨烯纳米片和金属纳米粒子装饰的石墨烯片是在氩气气氛下通过电弧放电法大量合成的。所合成的纳米结构通过不同的表征技术进行表征,例如XRD,SEM,TEM,能量色散X射线光谱,拉曼光谱和FTIR光谱。长度约6 cm的SWCNT纤网包含对齐的SWCNT,直径约为1.8 nm,并形成buckybook状结构。通过在变化的氩气气氛(250-500T)中对高纯度石墨电极进行电弧放电,可以制备出很少的石墨烯(FLG)片。在350T的氩气压力下,发现石墨烯的最大面积范围(具有最少的层数,即四层)。还报道了一种通过电弧放电法用铁和镍纳米粒子装饰这些石墨烯纳米片的一步方法。

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