Synthesis and characterization of some hydrous TPPTS center dot Ln complexes (Ln = Sc, Y, La, Nd, Sm, Gd, Ho; and TPPTS = TRIS(m-sulfonatophenyl)phosphine)

Chen XL.; Qiao QL.; Zhan L.; Yan SY.; Lei P.

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Synthesis and characterization of some hydrous TPPTS center dot Ln complexes (Ln = Sc, Y, La, Nd, Sm, Gd, Ho; and TPPTS = TRIS(m-sulfonatophenyl)phosphine)

机译：某些TPPTS水性中心点Ln配合物的合成和表征（Ln = Sc，Y，La，Nd，Sm，Gd，Ho; TPTPS = TRIS（间磺酰基苯基）膦）

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The TPPTS . Ln (Ln = Sc, Y, La, Nd, Sm, Gd, Ho; and TPPTS = tris (m-(sulfonatophenyl) phosphine) were synthesized from the precursor TPPTS . Na-3 and oxides of rare earth. The chemical composition of TPPTS . Ln was determined by elemental analysis and ICP-AES. The XPS showed that the sulfonate group in the complexes was coordinated with rare earth in a bridging tridentate manner. IR, Raman, P-31 NMR and TG-DTA graphs were recorded and discussed. (C) 1998 Elsevier Science Ltd. All rights reserved. [References: 23]

机译：TPPTS。 Ln（Ln = Sc，Y，La，Nd，Sm，Gd，Ho; TPPTS = tris（间-（磺酰基苯基）膦））是由前体TPPTS，Na-3和稀土氧化物合成的。用元素分析法和ICP-AES法测定TPPTS.Ln，XPS表明配合物中的磺酸根与稀土以三齿桥联方式结合，并记录了IR，拉曼，P-31 NMR和TG-DTA图谱。（C）1998 Elsevier Science Ltd.保留所有权利[参考文献：23]

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《Polyhedron: The International Journal for Inorganic and Organometallic Chemistry》 |1998年第8期|共5页
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Chen XL.; Qiao QL.; Zhan L.; Yan SY.; Lei P.;
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1. Synthesis and characterization of some hydrous TPPTS center dot Ln complexes (Ln = Sc, Y, La, Nd, Sm, Gd, Ho; and TPPTS = TRIS(m-sulfonatophenyl)phosphine) [J] . Chen XL., Qiao QL., Zhan L., Polyhedron: The International Journal for Inorganic and Organometallic Chemistry . 1998,第8期

机译：某些TPPTS水性中心点Ln配合物的合成和表征（Ln = Sc，Y，La，Nd，Sm，Gd，Ho; TPTPS = TRIS（间磺酰基苯基）膦）
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机译：异结构四核镧系元素[Ln _4（μ_3-OH）_2（ampdH _4）_2（piv）_（10）]·4CH _3CN的合成与表征（Ln = Sm，Eu，Gd，Tb，Dy，Ho，Er ）
4. A New Class Of Ln~(2+) Complexes, K(2.2.2-cryptand){Ln(OAr~(Ad'Me))_3mes}:Synthesis, Structure, Spectroscopy, and Theoretical Characterization [C] . Chad T Palumbo, Megan E. Fieser, Dominik P. Halter Rare Earth Research Conference . 2019

机译：一种新的LN〜（2+）复合物，K（2.2.2- Cryptand） {ln （oar〜（ad'me））_ 3mes}：合成，结构，光谱学和理论表征
5. Synthesis and characterization of iron complexes of tris-thiolate phosphine tripod ligands as models of the FeS(3) centers of nitrogenase and the Fe(CO)(CN)2 center of hydrogenase. [D] . Hsu, Hua-Fen. 1997

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6. Heterometallic Octanuclear NiII4LnIII4 (Ln = Y Gd Tb Dy Ho Er) ComplexesContaining NiII2LnIII2O4 Distorted Cubane Motifs: Synthesis Structure andMagnetic Properties [O] . Pankaj Kalita, Joydeb Goura, Juan Manuel Herrera, 2018

机译：杂金属八核NiII4LnIII4（Ln = YGdTbDyHoEr）配合物包含NiII2LnIII2O4扭曲的古巴图案：合成结构和磁性能
7. Template synthesis, crystal structure and luminescent properties of neutral N4O3 tripodal LnIIIL complexes (Ln III = La3+, Eu3+, Gd3+, Tb 3+, Dy3+, Ho3+, Er3+, Tm3+ or Lu3+; H3L = Tris{3′-(2″- pyridyl)-5′-tert-butyl-2′-hydroxybenzylidene-2-iminoethyl}amine) [O] . Wong WK, Liang H, Guo J, 2004

机译：中性N4O3三脚架LnIIIL配合物（Ln III = La3 +，Eu3 +，Gd3 +，Tb 3 +，Dy3 +，Ho3 +，Er3 +，Tm3 +或Lu3 +的模板合成，晶体结构和发光特性; H3L = Tris {3'-（2''-吡啶基）-5'-叔丁基-2'-羟基亚苄基-2-亚氨基乙基}胺）
8. Formation of Tetra-and Tri-nuclear Nickel Acetylene Complexes; Crystal and Molecular Structures of Tris-u3-(n-2-Hexafluorobut-2yne)-Tetrakis-(Carbonylnickel) and Orobut-2yne)-Tetrakis-(Carbonylnickel) and t-2-Yne)-Tetrakis-(Carbonylnickel) and Trakis-(Carbonylnickel) and El) and Tricarbonyl-u3-(n-Cyclo-Octatetraene)-u3-(n-2-Hexafluorobut-2-Yne)- Triangulo-Trinickel with Evidence for a Nickel-Stabilised Cyclo-Octatetraenyl Dication. [R] . Davidson, J. L., Green, M., Stone, F. G. A., 1978

机译：四核和三核镍乙炔配合物的形成; Tris-u3-（n-2-六氟丁-2-炔）-Tetrakis-（羰基镍）和Orobut-2yne）-Tetrakis-（羰基镍）和t-2-Yne）-Tetrakis-（羰基镍）和Trakis的晶体和分子结构 - （羰基镍）和E1）和三羰基-u3-（n-环 - 辛二烯）-u3-（n-2-六氟丁-2-炔） - 三羰基 - 三萜，具有镍稳定的环辛烯基四烯基二价的证据。

Synthesis and characterization of some hydrous TPPTS center dot Ln complexes (Ln = Sc, Y, La, Nd, Sm, Gd, Ho; and TPPTS = TRIS(m-sulfonatophenyl)phosphine)

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