Synthesis of macrocyclic tetrazoles for rapid photoinduced bioorthogonal 1,3-dipolar cycloaddition reactions

Yu Z.; Lim R.K.V.; Lin Q.

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Synthesis of macrocyclic tetrazoles for rapid photoinduced bioorthogonal 1,3-dipolar cycloaddition reactions

机译：合成大环四唑用于快速光诱导的生物正交1,3-偶极环加成反应

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Quick as a flash! A series of conformationally constrained, macrocyclic tetrazoles were expediently prepared by double alkylation of a bis(o-phenolyl)tetrazole precursor. Several of them showed excellent reactivity toward norbornene in a photoinduced tetrazole-alkene cycloaddition reaction in organic solvent, as well as toward a norbornene-modified protein in phosphate-buffered saline buffer (see scheme).

机译：快闪！通过双（邻-苯酚基）四唑前体的双烷基化方便地制备了一系列构象受限的大环四唑。其中一些在有机溶剂中在光诱导的四唑-烯烃环加成反应中对降冰片烯具有极好的反应性，在磷酸盐缓冲液中对降冰片烯修饰的蛋白质也具有极好的反应性（参见方案）。

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《Chemistry: A European journal》 |2010年第45期|共5页
作者
Yu Z.; Lim R.K.V.; Lin Q.;
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正文语种 eng
中图分类应用化学;
关键词
alkenes; bioorthogonal chemistry; biotechnology; cycloaddition; tetrazoles;

机译：烯烃;生物正交化学;生物技术;环加成;四唑;

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1. Synthesis of macrocyclic tetrazoles for rapid photoinduced bioorthogonal 1,3-dipolar cycloaddition reactions [J] . Yu Z., Lim R.K.V., Lin Q. Chemistry: A European journal . 2010,第45期

机译：合成大环四唑用于快速光诱导的生物正交1,3-偶极环加成反应
2. 5-(Methylthio)tetrazoles as versatile synthons in the stereoselective synthesis of polycyclic pyrazolines via photoinduced intramolecular nitrile imine-alkene 1,3-dipolar cycloaddition [J] . Daniel Pla, Derek S. Tan, David Y. Gin Chemical science . 2014,第6期

机译：5-（甲硫硫基）四唑作为多环吡唑啉的立体选择合成的多圆形合成，通过光致髓质淀粉胺，通过光致染色的分子内腈亚氨基烯-烯烃1,3-偶极环加装
3. Synthesis of some tetrazole fused pyrido[2,3-c]coumarin derivatives from a one-pot three-component reaction via intramolecular 1,3-dipolar cycloaddition reaction of azide to nitriles [J] . Pallabi Borah, P. Seetham Naidu, Pulak J. Bhuyan Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2012,第37期

机译：通过叠氮化物与腈的分子内1,3-偶极环加成反应由一锅三组分反应合成一些四唑稠合的吡啶并[2,3-c]香豆素衍生物
4. Synthesis of Nitrogen Heterocycles through 1,3-Dipolar Cycloaddition Reactions [C] . Simonetta Benetti, Carmela De Risi Edition of the A. Corbella" summer school on organic synthesis" . 1999

机译：通过1,3-偶极环加成反应合成氮杂环
5. Part I: 1,3,4-oxadiazoles in tandem Diels-Alder, 1,3-dipolar cycloaddition reactions: A rapid synthesis of vinca alkaloid motifs. Part II: Exceptionally potent inhibitors of fatty acid amide hydrolase [D] . Wilkie, Gordon David 2002

机译：第一部分：串联Diels-Alder中的1,3,4-恶二唑，1,3-偶极环加成反应：长春花生物碱基序的快速合成。第二部分：脂肪酸酰胺水解酶的超强抑制剂
6. Synthesis of Macrocyclic Tetrazoles for Rapid Photoinduced Bioorthogonal 13-Dipolar Cycloaddition Reactions [O] . Dr. Zhipeng Yu, Reyna K. V. Lim, Prof. Dr. Qing Lin -1

机译：用于快速光诱导的生物正交13-偶极环加成反应的致癌致四唑的合成
7. Macrocyclic Pendant Arm Extension: An Application of the Husigen 1,3-Dipolar Cycloaddition Reaction [O] . Kline Cory, Roesner Faculty Advisor Rebecca 2010

机译：大环吊坠臂延伸：Husigen 1,3-偶极环加成反应的应用

Synthesis of macrocyclic tetrazoles for rapid photoinduced bioorthogonal 1,3-dipolar cycloaddition reactions

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