Benign and Efficient Synthesis of 2-Substituted 4(3H)-Quinazolinones Mediated by Iron(III)Chloride Hexahydrate in Refluxing Water

Guan-Wu Wang; Chun-Bao Miao; Hui Kang

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Benign and Efficient Synthesis of 2-Substituted 4(3H)-Quinazolinones Mediated by Iron(III)Chloride Hexahydrate in Refluxing Water

机译：六水合氯化铁（III）介导的回流水中良性高效合成2-取代的4（3H）-喹唑啉酮

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Condensation of aldehydes with anthranilamide in refluxing water using iron(III)chloride hexahydrate as an oxidiant afforded 2-substituted 4(3H)-quinazolinones in good yields (77-93%).This method provides several advantages such as being environmentally friendly,having a simple work-up procedure,and affording high yields.

机译：使用六水合氯化铁（III）作为氧化剂，将乙醛与邻氨基苯甲酰胺在回流水中缩合，可制得2取代的4（3H）-喹唑啉酮，产率高（77-93％）。该方法具有以下优点：环保，具有简单的后处理程序，并提供高产量。

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《Bulletin of the Chemical Society of Japan》 |2006年第9期|共5页
作者
Guan-Wu Wang; Chun-Bao Miao; Hui Kang;
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中图分类化学;
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Benign and Efficient Synthesis of 2-Substituted 4(3H)-Quinazolinones Mediated by Iron(III)Chloride Hexahydrate in Refluxing Water

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