SYNTHESES AND CRYSTAL STRUCTURE ANALYSES OF TETRAALKYL PHOSPHONIUM, ARSONIUM, AND STIBONIUM TRIIODIDES [German]

Breunig HJ.; Ebert KH.; Lork E.; Denker M.

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SYNTHESES AND CRYSTAL STRUCTURE ANALYSES OF TETRAALKYL PHOSPHONIUM, ARSONIUM, AND STIBONIUM TRIIODIDES [German]

机译：四烷基磷，砷和三碘化锑的合成及晶体结构分析[德国]

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The reaction of Me4EI (E = P, As), Me3EtSbI, Me2Et2SbI, MeEt3SbI, or Et4SbI with I-2 in absence of solvent gives Me4PI3 (E = P , As), Me3EtSbI3, Me2Et2SbI3, MeEt3SbI3, or Et4SbI3. Me4SbI3 is formed in a reversible reaction by addition of I-2 to (Me4Sb)(3)I-8 or by reaction of a solution of Me4SbI in ethanol with It in benzene. The crystal structures of Me4EI3 (E = P, Sb), and Me3EtSbI3 and the syntheses of the novel compounds are reported. [References: 8]

机译：Me4EI（E = P，As），Me3EtSbI，Me2Et2SbI，MeEt3SbI或Et4SbI在没有溶剂的情况下与I-2反应生成Me4PI3（E = P，As），Me3EtSbI3，Me2Et2SbI3，MeEt3SbI3或Et3S。通过向（Me4Sb）（3）I-8中添加I-2或通过Me4SbI在乙醇中的溶液与它在苯中的反应，可逆反应形成Me4SbI3。报告了Me4EI3（E = P，Sb）和Me3EtSbI3的晶体结构以及新型化合物的合成。 [参考：8]

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《Zeitschrift fur Anorganische und Allgemeine Chemie》 |1997年第7期|共6页
作者
Breunig HJ.; Ebert KH.; Lork E.; Denker M.;
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中图分类化学;
关键词
Tetraalkyl phosphonium triiodide; Tetraalkyl arsonium triiodide; Tetraalkyl stibonium triiodide; Crystal structures;

机译：四烷基tri碘化物;四烷基ar碘化物;四烷基sti三碘化物;晶体结构;

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1. SYNTHESES AND CRYSTAL STRUCTURE ANALYSES OF TETRAALKYL PHOSPHONIUM, ARSONIUM, AND STIBONIUM TRIIODIDES [German] [J] . Breunig HJ., Ebert KH., Lork E., Zeitschrift fur Anorganische und Allgemeine Chemie . 1997,第7期

机译：四烷基磷，砷和三碘化锑的合成及晶体结构分析[德国]
2. Syntheses, structures and intermolecular interactions of tetraorganoammonium, -phosphonium and -stibonium dimethyl- and diphenyltetrahaloantimonates [J] . Breunig HJ, Koehne T, Moldovan O, Journal of Organometallic Chemistry . 2010,第9期

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SYNTHESES AND CRYSTAL STRUCTURE ANALYSES OF TETRAALKYL PHOSPHONIUM, ARSONIUM, AND STIBONIUM TRIIODIDES [German]

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