SYNTHESIS OF 2,3-DIHYDROBENZO[l,4]DIOXINS AND -OXAZINS VIA A DOMINO WACKER-HECK REACTION

Lutz F. Tietze; Kristina F. Wilckens; Sinem Yilmaz; Florian Stecker

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SYNTHESIS OF 2,3-DIHYDROBENZO[l,4]DIOXINS AND -OXAZINS VIA A DOMINO WACKER-HECK REACTION

机译：多米诺·瓦克-赫克反应合成2,3-二羟基联苯并[1,4]二恶英和-恶嗪

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An efficient and operationally simple domino Wacker-Heck reaction of allylic phenols and alpha,betalpha-unsaturated ketones as well as esters in the presence of catalytic amounts of Pd(TFA)2 and an oxidant for the synthesis of 2,3-dihydro-benzo[l,4]dioxins and 2,3-dihydrobenzo[l,4]oxazins is described. The necessary substrates are prepared by monoallylation of catechol derivatives and ortho-aminophenol.

机译：在催化量的Pd（TFA）2和氧化剂存在下合成2,3-二氢-苯并呋喃的反应中，烯丙基苯酚和α，betalpha-不饱和酮以及酯的有效且操作简单的多米诺Wacker-Heck反应描述了[1，4]二恶英和2，3-二氢苯并[1，4]恶嗪。通过邻苯二酚衍生物和邻氨基苯酚的单烯丙基化制备必要的底物。

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《Heterocycles: An International Journal for Reviews and Communications in Heterocyclic Chemistry》 |2006年第0期|共11页
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Lutz F. Tietze; Kristina F. Wilckens; Sinem Yilmaz; Florian Stecker;
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1. SYNTHESIS OF 2,3-DIHYDROBENZO[l,4]DIOXINS AND -OXAZINS VIA A DOMINO WACKER-HECK REACTION [J] . Lutz F. Tietze, Kristina F. Wilckens, Sinem Yilmaz, Heterocycles: An International Journal for Reviews and Communications in Heterocyclic Chemistry . 2006,第0期

机译：多米诺·瓦克-赫克反应合成2,3-二羟基联苯并[1,4]二恶英和-恶嗪
2. Synthesis and reductive reactions of 2,3-dioxo-2,3-dihydrobenzo-[b]furo[2,3-f]-, -[2,3-g]-, and -[3,2-e]indoles [J] . T. E. Khoshtariya, M. M. Matnadze, N. T. Mirziashvili, Chemistry of heterocyclic compounds . 2004,第11期

机译：2,3-二氧代-2,3-二氢苯并-[b]呋喃[2,3-f]-，-[2,3-g]-和-[3,2-e]吲哚的合成和还原反应
3. Enantioselective palladium-catalyzed total synthesis of vitamin E by employing a domino Wacker-Heck reaction [J] . Tietze LF, Stecker F, Zinngrebe J, Chemistry: A European journal . 2006,第34期

机译：通过多米诺骨牌Wacker-Heck反应对映选择性钯催化的维生素E的全合成
4. Synthesis and reactions of 2,3-diaryltetrazolium mesoionic compounds [C] . Mirai Nakata, Tsunehisa Hirashita 日本化学会春季年会講演予稿集 . 2018

机译：2,3-二芳基三唑鎓中碘化合物的合成与反应
5. 1. Matrix ESR study of radical cations of acyclic enedyne compounds. 2. A solid-phase synthesis and combinatorial approach to 2,3-dihydrobenzo[d]isothiazole 1,1-dioxide. 3. Synthesis of hyaluronic acid disaccharide and its c-linked analogue. [D] . Jiang, Bin. 1999

机译：1.无环烯炔化合物自由基阳离子的基质ESR研究。 2.2，3-二氢苯并[d]异噻唑1，1-二氧化物的固相合成和组合方法。 3.透明质酸二糖及其c-连接类似物的合成。
6. Front Cover: Synthesis of 4H‐Benzoe13oxazin‐4‐ones by a Carbonylation–Cyclization Domino Reaction of ortho‐Halophenols and Cyanamide (ChemistryOpen 5/2017) [O] . Linda Åkerbladh, Dr. Shiao Y. Chow, Dr. Luke R. Odell, 2017

机译：封面：邻卤代苯酚和氰胺的羰基化-环化多米诺反应合成4H-苯并e 13恶嗪-4-酮（ChemistryOpen 5/2017）
7. Synthesis of fused uracils: pyrano2,3-pyrimidines and 1,4-bis(pyrano2,3-pyrimidinyl)benzenes by domino Knoevenagel/Diels-Alder reactions [O] . 2012

机译：通过多米诺Knoevenagel / Diels-Alder反应合成吡喃并2,3-嘧啶和1,4-双（吡喃2,3-嘧啶基）苯

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SYNTHESIS OF 2,3-DIHYDROBENZO[l,4]DIOXINS AND -OXAZINS VIA A DOMINO WACKER-HECK REACTION

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