Syntheses and Thermal Properties of Poly(hydroxy)urethanes by Polyaddition Reaction of Bis(cyclic carbonate)and Diamines

Mi-Ra Kim; Hooi-Sung Kim; Chang-Sik Ha; Dae-Won Park; Jin-Kook Lee

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Syntheses and Thermal Properties of Poly(hydroxy)urethanes by Polyaddition Reaction of Bis(cyclic carbonate)and Diamines

机译：双（环状碳酸酯）与二胺的加成反应合成（羟基）氨基甲酸酯的合成及热性能

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In this study, we synthesized poly(hydroxy)urethanes by the polyaddition reaction of bis(cyclic carbonate) and diamine. Bis(cyclic carbonate) was prepared from diglycidyl ether based on bisphenol S and carbon dioxide. Thermal properties and solubilities of the poly(hydroxy)urethanes of five different diamines were compared. The thermal properties of the poly(hydroxy)urethanes depended on the structure of the diamine as well as the structure of the monomer. These poly(hydroxy)urethanes were soluble only in aprotic solvents because of the hydrophilic character of the hydroxy group.

机译：在这项研究中，我们通过双（环状碳酸酯）和二胺的加聚反应合成了聚（羟基）氨基甲酸酯。由基于双酚S和二氧化碳的二缩水甘油醚制备双（环状碳酸酯）。比较了五种不同二胺的聚（羟基）氨基甲酸酯的热性质和溶解度。聚（羟基）氨基甲酸酯的热性质取决于二胺的结构以及单体的结构。这些聚（羟基）氨基甲酸酯由于羟基的亲水性而仅可溶于非质子溶剂中。

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来源
《Journal of Applied Polymer Science》 |2001年第11期|共9页
作者
Mi-Ra Kim; Hooi-Sung Kim; Chang-Sik Ha; Dae-Won Park; Jin-Kook Lee;
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正文语种 eng
中图分类高分子化学（高聚物）;高分子化合物产品;有机化学;
关键词
poly(hydroxy)urethane; bis(cyclic carbonate); carbon dioxide; phase transfer catalyst;

机译：聚（羟基）氨基甲酸酯;双（环状碳酸酯）;二氧化碳;相转移催化剂;

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1. Syntheses and Thermal Properties of Poly(hydroxy)urethanes by Polyaddition Reaction of Bis(cyclic carbonate)and Diamines [J] . Mi-Ra Kim, Hooi-Sung Kim, Chang-Sik Ha, Journal of Applied Polymer Science . 2001,第11期

机译：双（环状碳酸酯）与二胺的加成反应合成（羟基）氨基甲酸酯的合成及热性能
2. Synthesis of polyhydroxyurethanes by ring-opening polyaddition of Bi-functional cyclic carbonates with diamines and the film properties [J] . Hidetoshi Tomita, Hiroyuki Hidaka, Fumio Sanda, 日本接着学会誌 . 2000,第7期

机译：双官能环状碳酸酯与二胺的开环加成反应合成聚羟基氨基甲酸酯及其薄膜性质
3. Synthesis of polyhydroxyurethanes by ring-opening polyaddition of Bi-functional cyclic carbonates with diamines and the film properties [J] . Hidetoshi Tomita, Hiroyuki Hidaka, Fumio Sanda, 日本接着学会誌 . 2000,第7期

机译：用二胺的双官能环碳酸酯的开环聚吡啶合成多羟基苯乙烷和膜性能
4. Synthesis of poly (hydroxyurethane)s from bis(cyclic carbonate) and diamine [C] . D.W.Park, J.Y.Moon The 4th Asian international conference of leather science and technology . 1998

机译：由双（环状碳酸酯）和二胺合成聚（羟基氨基甲酸酯）
5. MECHANISM OF THE REACTION OF CHLORO- AND 1,2-DICHLOROETHYLENE CARBONATE WITH PHENYLMAGNESIUM BROMIDE. SYNTHESIS OF THERMALLY STABLE IMIDE-CROSSLINKED POLY(4-VINYLPHTHALIC ANHYDRIDE), AND SYNTHESIS OF POLY(5-VINYL-8-HYDROXYQUINOLINE). [D] . VIJAYA RAGHAVAN, NADIPURAM V. 1968

机译：氯和1,2-二氯乙烯碳酸盐与苯甲基溴化镁反应的机理。热稳定的酰亚胺交联聚（4-乙烯基羟基酸酐）的合成，和聚（5-乙烯基-8-羟基喹啉）的合成。
6. Surface Properties of Poly(Hydroxyurethane)s Based on Five-Membered Bis-Cyclic Carbonate of Diglycidyl Ether of Bisphenol A [O] . Mariusz Tryznowski, Zuzanna Żołek-Tryznowska 2020

机译：基于双酚A的二元双环碳酸酯的聚（羟基氨基乙烷）S的表面性质
7. Synthesis and characterization of alternating poly(amide urea)s and poly(amide urethane urethane)s from ε-caprolactam, diamines, and diphenyl carbonate or ethylene carbonate [O] . Luc Ubaghs, Bhaskar Sharma, Helmut Keul, 2003

机译：ε-己内酰胺，二胺和二苯基酯或碳酸二苯基或碳酸二苯基或碳酸酯交替聚（酰胺脲）和聚（酰胺氨基甲酸酯氨基甲酸酯）的合成与表征

Syntheses and Thermal Properties of Poly(hydroxy)urethanes by Polyaddition Reaction of Bis(cyclic carbonate)and Diamines

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