The synthesis and crystal structure determination of phenyl 2-(3,4-dihydro-1(2H)naphthalenylidine)hydrazinecarboxylate and Phenyl (2,4-dichlorophenyl-methylene)hydrazinecarboxylate

Potter C.; Smith A.M.R.; Metz C.R.; Pennington W.T.; VanDerveer D.G.; Beam C.F.

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The synthesis and crystal structure determination of phenyl 2-(3,4-dihydro-1(2H)naphthalenylidine)hydrazinecarboxylate and Phenyl (2,4-dichlorophenyl-methylene)hydrazinecarboxylate

机译：2-（3,4-二氢-1（2H）萘联苯基）肼甲酸苯基酯和（2,4-二氯苯基-亚甲基）联苯甲酸苯基酯的合成及晶体结构测定

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(E)-Phenyl 2-(3,4-dihydro-1(2H)-naphthalenylidine) hydrazinecarboxylate and (E)-phenyl (2,4-dichlorophenylmethylene) hydrazinecarboxylate were prepared by the condensation of 1-tetralone or 2,4-dichlorobenzaldehyde with phenyl hydrazinecarboxylate. Crystals of C_(17)H_(16)N _2O_2 3 are monoclinic, C2/c, a = 17.763(4) ?, b = 8.353(2) ?, c = 40.233(8) ?, Z = 16, V = 5,839(2) ? ~3, R_1 = 0.0448 and wR_2 = 0.1104 for reflections with I>2σ(I). Crystals of C_(14)H_(10)N _2O_2Cl_2 5 are orthorhombic, P2_12 _12_1, a = 8.288(3) ?, b = 14.082(2)?, c = 23.788(5)?, Z = 8, V = 2,777(1) ? ~3, R1 = 0.0815 and wR_2 = 0.2006 for reflections with I>2σ(I). The molecular packing in the crystal for both compounds is the result of N-H?O hydrogen bonding.

机译：（E）-苯基2-（3,4-二氢-1（2H）-萘啶）肼甲酸甲酯和（E）-苯基（2,4-二氯苯基亚甲基）肼甲酸甲酯通过1-四氢萘酮或2,4-缩合反应制得二氯苯甲醛与肼苯甲酸甲酯。 C_（17）H_（16）N _2O_2 3的晶体是单斜晶的，C2 / c，a = 17.763（4）α，b = 8.353（2）α，c = 40.233（8）α，Z = 16，V = 5,839（2）？〜3，对于I>2σ（I）的反射，R_1 = 0.0448和wR_2 = 0.1104。 C_（14）H_（10）N _2O_2Cl_2 5的晶体是正交晶体，P2_12 _12_1，a = 8.288（3）α，b = 14.082（2）α，c = 23.788（5）α，Z = 8，V = 2,777 （1）？〜3，对于I>2σ（I）的反射，R1 = 0.0815和wR_2 = 0.2006。两种化合物在晶体中的分子堆积都是N-H2O氢键的结果。

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来源
《Journal of chemical crystallography》 |2010年第6期|共5页
作者
Potter C.; Smith A.M.R.; Metz C.R.; Pennington W.T.; VanDerveer D.G.; Beam C.F.;
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正文语种 eng
中图分类晶体学;
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(E)-carbophenoxyhydrazones; 1-Tetralone; 2; 4-Dichlorobenzaldehyde; Phenyl hydrazinecarboxylate;

机译：（E）-羧苯氧基hydr;1-四酮;2;4-二氯苯甲醛;苯基肼甲酸;

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The synthesis and crystal structure determination of phenyl 2-(3,4-dihydro-1(2H)naphthalenylidine)hydrazinecarboxylate and Phenyl (2,4-dichlorophenyl-methylene)hydrazinecarboxylate

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