The Synthesis and Crystal Structure of a Novel Pesticide Intermediates

He Zhipeng; Ren Tiegang; Li Yongzhe; Fang Xiaomin

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The Synthesis and Crystal Structure of a Novel Pesticide Intermediates

机译：新型农药中间体的合成与晶体结构

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A novel pesticide intermediates 3-(6-bromo-2-methyl-3-(methylsulfonyl)phenyl)-4,5-dihydroisoxazole was synthesized with 2,3-dimethylaniline as the starting materials. The final product and intermediates were characterized by mass spectra, H-1 NMR, infrared and elemental analysis. The crystal structure of compounds 6 and 8 were determined by single crystal X-ray diffraction. Results shown that two oxazole compounds crystallize in the monoclinic (6) and triclinic (8) with the space group of P 21/c for 6 and P-1 for 8, respectively.

机译：以2,3-二甲基苯胺为原料，合成了新型农药中间体3-（6-溴-2-甲基-3-（甲基磺酰基）苯基）-4,5-二氢异恶唑。最终产物和中间体通过质谱，H-1 NMR，红外和元素分析进行表征。通过单晶X射线衍射确定化合物6和8的晶体结构。结果表明，两种恶唑化合物在单斜晶（6）和三斜晶（8）中结晶，其空间群分别为P 21 / c为6和P-1为8。

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《Journal of chemical crystallography》 |2015年第9期|共8页
作者
He Zhipeng; Ren Tiegang; Li Yongzhe; Fang Xiaomin;
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原文格式 PDF
正文语种 eng
中图分类晶体学;
关键词
Synthesis; Characterization; Crystal structure; Pesticide intermediates; Oxazole;

机译：合成;表征;晶体结构;农药中间体;恶唑;

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1. The Synthesis and Crystal Structure of a Novel Pesticide Intermediates [J] . He Zhipeng, Ren Tiegang, Li Yongzhe, Journal of chemical crystallography . 2015,第8a9期

机译：新型农药中间体的合成与晶体结构
2. Synthesis and Crystal structure studies of Diethyl-(6-chloro-2-carbazolyl) Methyl malonate an intermediate in the synthesis of Anti-inflammatory drug Carprofen [J] . L. GaonkarSantosh, Mahendra M., NanjundaSwamy s, Research Journal of Pharmaceutical Sciences . 2012,第1期

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6. Crystal structures of DNA polymerase I capture novel intermediates in the DNA synthesis pathway [O] . Nicholas Chim, Lynnette N Jackson, Anh M Trinh, 2015

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7. Synthesis and Crystal structure studies of Diethyl-(6-chloro-2-carbazolyl) Methyl malonate an intermediate in the synthesis of Anti-inflammatory drug Carprofen [O] . Gaonkar S. L., Mahendra M., Nanjunda Swamy S., 2012

机译：丙二酸二乙酯-（6-氯-2-咔唑基）丙二酸甲酯的合成及晶体结构研究

The Synthesis and Crystal Structure of a Novel Pesticide Intermediates

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