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Deposition of iron nanoparticles onto multiwalled carbon nanotubes by helicon plasma-enhanced, chemical vapor deposition

机译:通过螺旋等离子体增强化学气相沉积法将铁纳米颗粒沉积到多壁碳纳米管上

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摘要

We report helicon plasma-enhanced, chemical vapor deposition (helicon-PECVD) of iron (Fe) nanoparticles onto multiwalled carbon nanotubes (MWCNTs) with ferrocene as an iron source. Ferrocene was evaporated from the bubbler by heating, and the helicon plasma treatment was performed with the evaporated ferrocene and hydrogen gas at (-)DC bias voltage. The resulting MWCNT/Fe nanoparticle hybrids were characterized by X-ray fluorescence spectroscopy, X-ray diffraction spectroscopy, field-emission scanning electron microscopy, transmission electron microscopy, micro-Raman spectroscopy, and superconducting quantum interference device magnetometry. (c) 2007 Elsevier B.V. All rights reserved.
机译:我们报告铁(Fe)纳米粒子到以二茂铁为铁源的多壁碳纳米管(MWCNT)上的螺旋等离子体增强化学气相沉积(helicon-PECVD)。通过加热从鼓泡器中蒸发出二茂铁,并且在(-)DC偏压下用蒸发的二茂铁和氢气进行了螺旋等离子体处理。所得的MWCNT / Fe纳米粒子杂化物通过X射线荧光光谱,X射线衍射光谱,场发射扫描电子显微镜,透射电子显微镜,显微拉曼光谱和超导量子干涉装置磁力测定法进行表征。 (c)2007 Elsevier B.V.保留所有权利。

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