Cross-coupling reaction between arylboronic acids and carboranyl iodides catalyzed by graphene oxide (GO)-supported Pd(0) recyclable nanoparticles for the synthesis of carboranylaryl ketones?

Algin Oh Biying; Venu R. Vangala; Chia Sze Chen; Ludger Paul Stubs; Narayan S. Hosmane; Zhu Yinghuai

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Cross-coupling reaction between arylboronic acids and carboranyl iodides catalyzed by graphene oxide (GO)-supported Pd(0) recyclable nanoparticles for the synthesis of carboranylaryl ketones?

机译：氧化石墨烯（GO）负载的Pd（0）可循环利用纳米粒子催化的芳基硼酸和碳硼烷基碘化物之间的交叉偶联反应，用于合成碳硼烷基芳基酮？

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摘要

Well-dispersed palladium(0) nanoparticles with small and narrow size distributions were synthesized conveniently on a graphene oxide (GO) surface. The GO-supported nano-Pd~0 was found to be a highly efficient and recyclable catalyst for the carbonylative cross-coupling reaction between arylboronic acids and aryl and carboranyl iodides, respectively. Benzophenone and a series of carboranylaryl ketones, 1-R-2-[C(vO)Ar]-1,2-C_2B_(10)H_(10) (R = H, Me, Ph; Ar = C_6H_5, C_6H_4-4-OMe and C_6H_4-4-F), were synthesized and fully characterized. The catalyst was recyclable at least three times with sustained activity.

机译：可以在氧化石墨烯（GO）表面方便地合成具有小而窄尺寸分布的分散良好的钯（0）纳米颗粒。已发现GO负载的纳米Pd〜0是一种高效且可回收的催化剂，可分别用于芳基硼酸与芳基和碳硼烷基碘化物之间的羰基交叉偶联反应。二苯甲酮和一系列碳硼烷基芳基酮，1-R-2- [C（vO）Ar] -1,2-C_2B_（10）H_（10）（R = H，Me，Ph; Ar = C_6H_5，C_6H_4-4 -OMe和C_6H_4-4-F）被合成并充分表征。该催化剂可循环使用至少三遍，并具有持续的活性。

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《Dalton transactions: An international journal of inorganic chemistry》 |2014年第13期|共7页
作者
Algin Oh Biying; Venu R. Vangala; Chia Sze Chen; Ludger Paul Stubs; Narayan S. Hosmane; Zhu Yinghuai;
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正文语种 eng
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carbonylative; distributions; carboranylaryl;

机译：羰基;分布;碳烷基芳基;

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1. Cross-coupling reaction between arylboronic acids and carboranyl iodides catalyzed by graphene oxide (GO)-supported Pd(0) recyclable nanoparticles for the synthesis of carboranylaryl ketones? [J] . Algin Oh Biying, Venu R. Vangala, Chia Sze Chen, Dalton transactions: An international journal of inorganic chemistry . 2014,第13期

机译：氧化石墨烯（GO）负载的Pd（0）可循环利用纳米粒子催化的芳基硼酸和碳硼烷基碘化物之间的交叉偶联反应，用于合成碳硼烷基芳基酮？
2. Cross-coupling reaction between arylboronic acids and carboranyl iodides catalyzed by graphene oxide (GO)-supported Pd(0) recyclable nanoparticles for the synthesis of carboranylaryl ketones? [J] . Algin Oh Biying, Venu R. Vangala, Chia Sze Chen, Dalton transactions: An international journal of inorganic chemistry . 2014,第13期

机译：氧化石墨烯（GO）负载的Pd（0）可循环利用纳米粒子催化的芳基硼酸和碳硼烷基碘化物之间的交叉偶联反应，用于合成碳硼烷基芳基酮？
3. Green Synthesis of Pd Nanoparticles Supported on Magnetic Graphene Oxide by Origanum vulgare Leaf Plant Extract: Catalytic Activity in the Reduction of Organic Dyes and Suzuki–Miyaura Cross-Coupling Reaction [J] . Neda Seyedi, Kazem Saidi, Hassan Sheibani Catalysis Letters . 2018,第1期

机译：通过<重点型=“斜体”氧化物支持磁性石墨烯的Pd纳米颗粒的绿色合成overanum vulgare 叶植物提取物：催化活性在减少有机染料和铃木 - Miyaura交叉偶联反应中的催化活性
4. Chiral Rhodium Nanoparticle-catalyzed Asymmetric 1,4- Addition Reactions of Arylboronic Acids with β,γ-Unsaturated α-Ketocarbonyl Compounds [C] . Zhiyuan ZHU, Hiroyuki MIYAMURA, Tomohiro YASUKAWA 日本化学会春季年会講演予稿集 . 2018

机译：手性铑纳米粒子催化的不对称1,4-添加芳基硼酸与β，γ-不饱和α-酮烷基化合物的反应
5. Part I Expansion of Type II Anion Relay Chemistry (ARC); Part II Synthesis of a Recyclable Polymer-Supported Siloxane Transfer Agent for Transition Metal-Catalyzed Cross-Coupling Reactions (CCR) of Organolithiums [D] . O'Brien, Kevin T. 2020

机译：第一部分扩张II型阴离子继电器化学（弧）;第二部分合成过渡金属催化的硅氧烷转移剂的可再循环聚合物负载硅氧烷转移剂（CCR）的有机锂
6. Suzuki–Miyaura cross-coupling reaction of 1-aryltriazenes with arylboronic acids catalyzed by a recyclable polymer-supported N-heterocyclic carbene–palladium complex catalyst [O] . Guangming Nan, Fang Ren, Meiming Luo 2010

机译：可回收的聚合物负载的N-杂环卡宾-钯配合物催化的1-芳基三氮烯与芳基硼酸的铃木-宫浦交叉偶联反应
7. Synthesis of unsymmetrical biaryl ketones via palladium-catalyzed carbonylative cross-coupling reaction of arylboronic acids with iodoarenes [O] . Ishiyama, Tatsuo, Kizaki, Hiroe, Miyaura, Norio, 1993

机译：通过芳基硼酸与碘代芳烃的钯催化羰基交叉偶联反应合成不对称联芳基酮

Cross-coupling reaction between arylboronic acids and carboranyl iodides catalyzed by graphene oxide (GO)-supported Pd(0) recyclable nanoparticles for the synthesis of carboranylaryl ketones?

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