首页> 外文期刊>Journal of Applied Polymer Science >Measuring interdiffusion at an interface between two elastomers with tapping-mode and contact-resonance atomic force microscopy Imaging
【24h】

Measuring interdiffusion at an interface between two elastomers with tapping-mode and contact-resonance atomic force microscopy Imaging

机译:用敲击模式和接触共振原子力显微镜成像法测量两个弹性体之间界面的互扩散

获取原文
获取原文并翻译 | 示例
           

摘要

Despite the common use of tapping-mode atomic force microscopy to image composites or polymer blends, very few studies have focused on the measurement of the interdiffusion at an interface between two polymers in contact. In this study, we show how to assess the interphase between two polymers with two methods. First, stable and robust tapping conditions are established, and the problem of the phase contrast is discussed. Second, a contact-resonance method is presented: the tip in contact with the sample is electrostatically excited at its resonance frequency by a self-controlled oscillator. The gain and frequency images allow us to measure the interdiffusion width. Both methods (using high and weak mechanical solicitation) give the same assessment of the interdiffusion width. (c) 2008 Wiley Periodicals, Inc.
机译:尽管通常使用敲击模式原子力显微镜对复合材料或聚合物共混物进行成像,但很少有研究集中在两种接触聚合物之间界面处互扩散的测量上。在这项研究中,我们展示了如何使用两种方法评估两种聚合物之间的界面。首先,建立稳定和鲁棒的抽头条件,并讨论相衬问题。其次,提出了一种接触共振方法:与样品接触的尖端由自控振荡器以其共振频率进行静电激发。增益和频率图像使我们能够测量互扩散宽度。两种方法(使用高机械强度和弱机械强度)对互扩散宽度进行了相同的评估。 (c)2008年Wiley Periodicals,Inc.

著录项

相似文献

  • 外文文献
  • 中文文献
  • 专利
获取原文

客服邮箱:kefu@zhangqiaokeyan.com

京公网安备:11010802029741号 ICP备案号:京ICP备15016152号-6 六维联合信息科技 (北京) 有限公司©版权所有
  • 客服微信

  • 服务号