Enzymatic approach to cascade synthesis of bis(indolyl)methanes in pure water

Fu Yajie; Lu Zeping; Fang Ke; He Xinyi; Xu Huajin; Hu Yi

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Enzymatic approach to cascade synthesis of bis(indolyl)methanes in pure water

机译：酶促方法在纯水中级联合成双（吲哚基）甲烷

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A mild, efficient, and green protocol was developed for the synthesis of bis(indolyl)methanes catalyzed by lipase TLIM through the cascade reactions of indole with aldehydes in pure water. This methodology offers many superiorities such as excellent yields, wide substrate range, simple procedure, reusable and minimal amount of catalyst, and the ability to be scaled up.

机译：开发了一种温和，有效和绿色的方案，用于通过吲哚与纯水中的醛醛酸的级联反应合成脂肪酶TLIM催化的双（吲哚基）甲烷。该方法提供了许多优异的产量，宽基板范围，简单的过程，可重复使用和最小量的催化剂，以及缩小的能力。

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《RSC Advances》 |2020年第18期|共6页
作者
Fu Yajie; Lu Zeping; Fang Ke; He Xinyi; Xu Huajin; Hu Yi;
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Nanjing Tech Univ Sch Pharmaceut Sci State Key Lab Mat Oriented Chem Engn Nanjing 210009 Peoples R China;

Nanjing Tech Univ Sch Pharmaceut Sci State Key Lab Mat Oriented Chem Engn Nanjing 210009 Peoples R China;

Nanjing Tech Univ Sch Pharmaceut Sci State Key Lab Mat Oriented Chem Engn Nanjing 210009 Peoples R China;

Nanjing Tech Univ Sch Pharmaceut Sci State Key Lab Mat Oriented Chem Engn Nanjing 210009 Peoples R China;

Nanjing Tech Univ Sch Pharmaceut Sci State Key Lab Mat Oriented Chem Engn Nanjing 210009 Peoples R China;

Nanjing Tech Univ Sch Pharmaceut Sci State Key Lab Mat Oriented Chem Engn Nanjing 210009 Peoples R China;

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正文语种 eng
中图分类化学;
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1. Enzymatic approach to cascade synthesis of bis(indolyl)methanes in pure water [J] . Fu Yajie, Lu Zeping, Fang Ke, RSC Advances . 2020,第18期

机译：酶促方法在纯水中级联合成双（吲哚基）甲烷
2. Poly(N,N'-dichloro-N-ethyl-benzene-1, 3-disulfonamide) and N,N,N',N'-tetrachlorobenzene-1,3-disulfonamide as novel catalytic reagents for synthesis of bis-indolyl, tris-indolyl, di(bis-indolyl), tri(bis-indolyl) and tetra(bis-indolyl)methanes under solid-state, solvent and water conditions [J] . Hojat Veisi, Ramin Ghorbani-vaghei Journal of the Brazilian Chemical Society . 2010,第2期

机译：聚（N，N'-二氯-N-乙基苯-1,3-二磺酰胺）和N，N，N'，N'-四氯苯-1,3-二磺酰胺为合成双吲哚基的新型催化试剂，固态，溶剂和水条件下的三吲哚基甲烷，二（双吲哚基），三（双吲哚基）和四（双吲哚基）甲烷
3. Poly(N,N'-dichloro-N-ethyl-benzene-1, 3-disulfonamide) and N,N,N',N'-Tetrachlorobenzene-1,3-disulfonamide as Novel Catalytic Reagents for Synthesisof Bis-indolyl, Tris-indolyl, Di(bis-indolyl), Tri(bis-indolyl) and Tetra(bis-indolyl)Methanes under Solid-State, Solvent and Water Conditions [J] . Ramin Ghorbani-Vaghei, Hojat Veisi Journal of the Brazilian Chemical Society . 2010,第2期

机译：聚（N，N'-二氯-N-乙基苯-1,3-二磺酰胺）和N，N，N'，N'-四氯苯-1,3-二磺酰胺作为合成双吲哚基，Tris的新型催化试剂固态，溶剂和水条件下的-吲哚基，二（双-吲哚基），三（双-吲哚基）和四（双-吲哚基）甲烷
4. Ultrasound-assisted green synthesis of bis(indolyl)methanes catalyzed by acidic Ionic liquid (CH2)4SO4HMIMHSO4 [C] . Yingming Mo, Hongjun Zang, Bowen Cheng 2010 International Conference on Mechanic Automation and Control Engineering . 2010

机译：酸性离子液体（CH 2 ） 4 SO 4 HMIM HSO <的超声辅助绿色合成双（吲哚基）甲烷inf> 4
5. Cytotoxicity of indole-ring substituted 1,1-bis (3'-indolyl)-1-(p-phenyl-t-butyl) methanes in colon cancer cells [D] . Newman, Kristin Laine. 2008

机译：吲哚环取代的1,1-双（3'-吲哚基）-1-（对苯基叔丁基）甲烷在结肠癌细胞中的细胞毒性
6. Synthesis of Bis(indolyl)methanes Using Hyper-Cross-LinkedPolyaromatic Spheres Decorated with Bromomethyl Groups as Efficientand Recyclable Catalysts [O] . ReddiMohan Naidu Kalla, Sung Chul Hong, *, 2018

机译：超交联法合成双（吲哚基）甲烷高效装饰有溴甲基基团的多芳烃球和可循环使用的催化剂
7. Enzymatic approach to cascade synthesis of bis(indolyl)methanes in pure water [O] . Yajie Fu, Zeping Lu, Ke Fang, 2020

机译：酶促方法在纯水中级联合成双（吲哚基）甲烷

Enzymatic approach to cascade synthesis of bis(indolyl)methanes in pure water

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