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Exploring the Fundamentals of Microreactor Technology with Multidisciplinary Lab Experiments Combining the Synthesis and Characterization of Inorganic Nanoparticles

机译:用多学科实验室实验探索微反应器技术的基础,结合无机纳米粒子的合成和表征

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摘要

Multidisciplinary lab experiments combining microfluidics, nano particle synthesis, and characterization are presented. These experiments rely on the implementation of affordable yet efficient microfluidic setups based on perfluoroalkoxyalkane (PFA) capillary coils and standard HPLC connectors in upper undergraduate chemistry laboratories. Fundamental principles and concepts as well as practical tips for the rapid deployment of microfluidics are presented. In line membrane separation, the segmented-flow regime, high-temperature experiments, and in-line analytical techniques are illustrated by the preparation of inorganic nanoparticles (silver, gold, and cadmium selenide or telluride) in microreactors. Besides microfluidics, analytical techniques for nanoparticle analysis are also illustrated.
机译:介绍了微流体,纳米颗粒合成和表征的多学科实验室实验。 这些实验依赖于基于全氟烷氧氧烷(PFA)毛细管线圈和标准HPLC连接器的实惠且有效的微流体设置的实惠的实惠,在上本科化学实验室中的标准HPLC连接器。 提出了基本原则和概念以及快速部署微流体的实用提示。 在线膜分离中,通过在微反应器中制备无机纳米粒子(银,金和硒化镉或碲化酰胺)来说明分段流动状态,高温实验和在线分析技术。 除了微流体外,还示出了纳米粒子分析的分析技术。

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