New route to 1,4-oxazepane and 1,4-diazepane derivatives: synthesis from N-propargylamines

Vessally Esmail; Hosseinian Akram; Edjlali Ladan; Bekhradnia Ahmadreza; Esrafili Mehdi D.

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New route to 1,4-oxazepane and 1,4-diazepane derivatives: synthesis from N-propargylamines

机译：1,4-氧己烷和1,4-二氮杂己烷衍生物的新途径：来自N-丙氨酸的合成

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N-Propargylamines are one of the most useful and versatile building blocks in organic synthesis that are successfully transformed into many significant N-heterocycles. Due to high atom economy and shorter synthetic routes, the synthesis of 1,4-oxazepane and 1,4-diazepane cores from N-propargylamines have undergone an explosive growth in recent years. This review gives an overview of new developments in the synthesis of the title compounds from N-propargylamines in recent years. Mechanistic aspects of the reactions are considered and discussed in detail.

机译：N-丙基吡喃胺是有机合成中最有用和多功能的构建块之一，其成功地转化为许多显着的N-杂环。由于原子经济高，合成途径较短，近年来，来自N-丙基胺的1,4-氧己烷和1,4-二氮杂甲烷核的合成经历了爆炸性的增长。近年来，本综述概述了来自N-丙氨酸的标题化合物的合成。考虑并详细讨论反应的机械方面。

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来源
《RSC Advances》 |2016年第102期|共13页
作者
Vessally Esmail; Hosseinian Akram; Edjlali Ladan; Bekhradnia Ahmadreza; Esrafili Mehdi D.;
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作者单位

Payame Noor Univ Dept Chem Tehran Iran;

Univ Tehran Coll Engn Dept Engn Sci POB 11365-4563 Tehran Iran;

Islamic Azad Univ Tabriz Branch Dept Chem Tabriz Iran;

Mazandaran Univ Med Sci Dept Med Chem Pharmaceut Sci Res Ctr Sari Iran;

Univ Maragheh Dept Chem Maragheh Iran;

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正文语种 eng
中图分类化学;
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1. New route to 1,4-oxazepane and 1,4-diazepane derivatives: synthesis from N-propargylamines [J] . Vessally Esmail, Hosseinian Akram, Edjlali Ladan, RSC Advances . 2016,第102期

机译：1,4-氧己烷和1,4-二氮杂己烷衍生物的新途径：来自N-丙氨酸的合成
2. Synthesis of analogs of (1,4)-3- and 5-imino oxazepane, thiazepane, and diazepane as inhibitors of nitric oxide synthases. [J] . Wong KK Bioorganic and Medicinal Chemistry Letters . 2004,第23期

机译：合成（1,4）-3-和5-亚氨基氧杂环庚烷，噻嗪烷和二氮杂庚烷作为一氧化氮合酶的抑制剂。
3. Synthesis of analogs of (1,4)-3- and 5-imino oxazepane, thiazepane, and diazepane as inhibitors of nitric oxide synthases. [J] . Wong KK Bioorganic and Medicinal Chemistry Letters . 2004,第23期

机译：合成（1,4）-3-和5-亚氨基氧杂环庚烷，噻嗪烷和二氮杂庚烷作为一氧化氮合酶的抑制剂。
4. Utilization of Cinnamaldehyde for Synthesis of Nitrogencontaining 2-Hydroxy-1,4-Naphthoquinone Derivatives as Antioxidant Agent [C] . N. Nurhikmah, A. H. Cahyana, A. R. Liandi International Symposium on Current Progress in Mathematics and Sciences . 2020

机译：用利用肉桂醛的合成硝基因特突出的2-羟基-1,4-萘醌衍生物作为抗氧化剂
5. Synthesis of side chain-modified iodothyronines. Synthesis and structure-activity relationships (SARS) of galanthamine derivatives. Total synthesis of (+)-valyldetoxinine. Synthesis and mechanism of cyclic acetal and ketal formation in pentono-1,4-lactones. [D] . Han, So-Yeop. 1992

机译：侧链修饰的碘甲状腺素的合成。加兰他敏衍生物的合成及其构效关系（SARS）。（+）-Valyldetoxinine的全合成。戊通-1,4-内酯中环状缩醛和缩酮的合成及其机理。
6. 1,4-Ditosyl-1,4-diazepane [O] . Shuang-Hua Yang, Zhi-Wei Zhai 2015

机译：1,4-二甲苯基-1,4-二氮杂pan
7. 7-Endo selenocyclization reactions on chiral 3-prenyl and 3-cinnamyl-2 hydroxymethylperhydro-1,3-benzoxazine derivatives. A way to enantiopure 1,4-oxazepanes [O] . Nieto Román Francisco Javier, Andrés Juan Celia, Pérez-Encabo Alfonso 2015

机译：手性3-异戊烯基和3-肉桂基-2羟甲基过氢-1,3-苯并恶嗪衍生物的7-内烯基硒环化反应。对映体纯的1,4-恶唑酮的方法

New route to 1,4-oxazepane and 1,4-diazepane derivatives: synthesis from N-propargylamines

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