Metal-Free Benzannulation to Synthesis of 2,3-Disubstituted Naphthalenes: Reaction of 2-(Phenylethynyl)benzaldehyde and Alkynes by Bronsted Acid

Umeda Rui; Ikeda Naoki; Ikeshita Masahiro; Sumino Keita; Nishimura Sota; Nishiyama Yutaka

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Metal-Free Benzannulation to Synthesis of 2,3-Disubstituted Naphthalenes: Reaction of 2-(Phenylethynyl)benzaldehyde and Alkynes by Bronsted Acid

机译：合成2,3-二取代的萘的无金属苯并：2-（苯基乙炔基）苯甲醛和炔烃的反应

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Metal-free benzannulation reaction of 2-(phenylethynyl)benzaldehyde and alkynes proceeded in the presence of Bronsted acid under microwave irradiation to give the 2,3-disubstituted naphthalenes.

机译：2-（苯基乙炔基）Benzaldehyde和炔烃的无金属苯均匀反应在微波辐射下在勃朗酸存在下进行，得到2,3-二取代的萘甲苯。

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《Bulletin of the Chemical Society of Japan》 |2017年第2期|共3页
作者
Umeda Rui; Ikeda Naoki; Ikeshita Masahiro; Sumino Keita; Nishimura Sota; Nishiyama Yutaka;
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Kansai Univ Fac Chem Mat &

Bioengn Osaka 5648680 Japan;

Kansai Univ Fac Chem Mat &

Bioengn Osaka 5648680 Japan;

Kansai Univ Fac Chem Mat &

Bioengn Osaka 5648680 Japan;

Kansai Univ Fac Chem Mat &

Bioengn Osaka 5648680 Japan;

Kansai Univ Fac Chem Mat &

Bioengn Osaka 5648680 Japan;

Kansai Univ Fac Chem Mat &

Bioengn Osaka 5648680 Japan;

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正文语种 eng
中图分类化学;
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1. Metal-Free Benzannulation to Synthesis of 2,3-Disubstituted Naphthalenes: Reaction of 2-(Phenylethynyl)benzaldehyde and Alkynes by Bronsted Acid [J] . Umeda Rui, Ikeda Naoki, Ikeshita Masahiro, Bulletin of the Chemical Society of Japan . 2017,第2期

机译：合成2,3-二取代的萘的无金属苯并：2-（苯基乙炔基）苯甲醛和炔烃的反应
2. Metal-free selective synthesis of 2-substituted benzimidazoles catalyzed by Bronsted acidic ionic liquid: Convenient access to one-pot synthesis of N-alkylated 1,2-disubstituted benzimidazoles [J] . Senapak Warapong, Saeeng Rungnapha, Jaratjaroonphong Jaray, Tetrahedron . 2019,第26期

机译：无金属选择性合成2-取代的苯并咪唑催化的铜酸性离子液体：方便进入N-烷基化1,2-二取代苯并咪唑的单罐合成
3. Cyclisation reaction between 3-methylquinoxaline-2-thione and benzaldehydes into 3-benzyl-2-aryl-thieno[2,3-b] quinoxaline promoted by Bronsted acids [J] . Saoudi Besma, Teniou Abderrahmane, Debache Adbelmadjid, Comptes Rendus Chimie . 2015,第8期

机译：3-甲基喹喔啉-2-硫酮与苯甲醛之间的环化反应为布朗斯台德酸促进的3-苄基-2-芳基-硫代[2,3-b]喹喔啉
4. Multistep Microwave-Assisted Solvent-Free Organic Reactions: Synthesis of 1,6-Disubstituted-4-Oxo-1,4-Dihydro-Pyridine-3-Carboxylic Acid Benzyl Esters [C] . Mauro Panunzio, Maria Antonietta Lentini, Eileen Campana, International Conference on Microwave and High Frequency Heating . 2006

机译：多步微波辅助溶剂有机反应：1,6-二取代-4-氧代-1,4-二氢 - 吡啶-3-羧酸苄基酯的合成
5. Part I. Synthesis of cytochrome P450-CAM substrate analogues towards developing cytochrome P450-CAM as an enzyme-based model system for mechanistic studies of important types of P450 reactions. Part II. Diels-Alder approach towards the synthesis of 2,3-disubstituted anthracene derivatives for luminescence spectroscopy characterization: Synthesis towards fluorescent sensors. [D] . Kemnitzer, William Edward. 1998

机译：第一部分。合成细胞色素P450-CAM底物类似物，以开发细胞色素P450-CAM作为一种基于酶的模型系统，用于重要类型P450反应的机理研究。第二部分Diels-Alder合成2,3-二取代蒽衍生物以进行发光光谱表征的方法：合成荧光传感器。
6. Synthesis of Naphthalenes through Three-Component Coupling of Alkynes Fischer Carbene Complexes and Benzaldehyde Hydrazones via Isoindole Intermediates [O] . Shaofeng Duan, Dilip K. Sinha-Mahapatra, James W. Herndon -1

机译：通过异吲哚中间体通过炔烃费歇尔卡宾配合物和苯甲醛Hy的三组分偶联合成萘
7. Metal-Free Benzannulation to Synthesis of 2,3-Disubstituted Naphthalenes: Reaction of 2-(Phenylethynyl)benzaldehyde and Alkynes by Brønsted Acid [O] . UMEDA Rui, IKEDA Naoki, IKESHITA Masahiro, 2017

机译：无金属苯环合成2,3-二取代萘的合成：布朗斯台德酸与2-（苯基乙炔基）苯甲醛和炔烃的反应

Metal-Free Benzannulation to Synthesis of 2,3-Disubstituted Naphthalenes: Reaction of 2-(Phenylethynyl)benzaldehyde and Alkynes by Bronsted Acid

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