Solvothermal Synthesis and Surface Chemistry To Control the Size and Morphology of Nanoquartz

Sochalski-Kolbus Lindsay M.; Wang Hsui-Wen; Rondinone Adam J.; Anovitz Lawrence M.; Wesolowski David J.; Whitfield Pamela S.

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Solvothermal Synthesis and Surface Chemistry To Control the Size and Morphology of Nanoquartz

机译：溶剂热合成和表面化学以控制纳米石英的尺寸和形态

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In this work, we report a solvothermal synthesis method that allows the crystallization of quartz to occur at a relatively low temperature of 300 degrees C in the form of isolated nanosized euhedral crystals. Transmission electron microscopy (TEM) and small area electron diffraction (SAED) were used to confirm the phases present and their particle sizes, morphologies, and crystallinity of the products. The results show that it is possible to control the size and morphology of the nanoquartz from rough nanospheres to nanorods using fluoride, which templates the nanocrystals and moderates growth.

机译：在这项工作中，我们报告了一种溶剂热合成方法，该方法允许石英的结晶以相对较低的300摄氏度的分离的纳米面体晶体的形式在相对较低的温度下发生。使用透射电子显微镜（TEM）和小面积电子衍射（SAED）确认存在的相及其产物的粒径，形态和结晶度。结果表明，使用氟化物可以控制从粗糙的纳米球到纳米棒的纳米石英的尺寸和形态，氟化物可以模板化纳米晶体并缓和生长。

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《Crystal growth & design》 |2015年第11期|共5页
作者
Sochalski-Kolbus Lindsay M.; Wang Hsui-Wen; Rondinone Adam J.; Anovitz Lawrence M.; Wesolowski David J.; Whitfield Pamela S.;
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正文语种 eng
中图分类晶体学;
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1. Solvothermal Synthesis and Surface Chemistry To Control the Size and Morphology of Nanoquartz [J] . Sochalski-Kolbus Lindsay M., Wang Hsui-Wen, Rondinone Adam J., Crystal growth & design . 2015,第11期

机译：溶剂热合成和表面化学以控制纳米石英的尺寸和形态
2. Combining complexing agent and solvothermal reaction for the morphology controlled synthesis of (Y,Eu)PO4 crystals with size-dependent photoluminescence [J] . Wang Zhihao, Wang Xuejiao, Takei Toshiaki, CrystEngComm . 2018,第32期

机译：用尺寸依赖性光致发光的（Y，E，欧盟）PO4晶体的形态控制合成的络合剂和溶剂热反应组合
3. Facile synthesis of morphology and size-controlled alpha-Fe2O3 and Fe3O4 nano-and microstructures by hydrothermal/solvothermal process: The roles of reaction medium and urea dose [J] . Su Minhua, He Chun, Shih Kaimin CERAMICS INTERNATIONAL . 2016,第13期

机译：水热/溶剂热法容易地合成形貌和尺寸受控的α-Fe2O3和Fe3O4纳米及微观结构：反应介质和尿素用量的作用
4. SOLVOTHERMAL SYNTHESIS OF NANO/MICRO-SIZED SODIUM NIOBATE POWDERS WITH TUNABLE MORPHOLOGIES [C] . QILIN GU, KONGJUN ZHU, LIUJING SONG, IUPAC 10th International conference on novel materials and their synthesis: Book of abstracts . 2014

机译：形态可调的纳米/微粉化铌酸钠粉末的溶剂热合成
5. Controlling Chemical Modification of Chlorinated Silicon Surfaces Via Wet-Chemistry Approaches and Morphology-Preserving Functionalization of Metal Oxide Nanomaterials Through Two-Step Click Reaction [D] . ?He, Chuan 2020

机译：通过两步咔哒反应控制通过湿化化学方法和金属氧化物纳米材料的形态保护官能化的化学改性。通过两步咔哒反应
6. Stabilization of Size-Controlled BaTiO3 Nanocubes viaPrecise Solvothermal Crystal Growth and Their AnomalousSurface Compositional Reconstruction [O] . Kouichi Nakashima, *, Kaito Onagi, 2021

机译：通过尺寸控制的BATIO3纳米核稳定精确的溶剂热晶体生长及其异常表面成分重建
7. Surface modification of TiO2 nanocrystals by WOx coating or wrapping: Solvothermal synthesis and enhanced surface chemistry [O] . Epifani, Mauro, Genç, Aziz, Arbiol, Jordi, 2016

机译：通过WOx涂层或包裹法对TiO2纳米晶体进行表面改性：溶剂热合成和增强的表面化学

Solvothermal Synthesis and Surface Chemistry To Control the Size and Morphology of Nanoquartz

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