Synthesis, Crystal Structure, and Antibacterial Activity of Di-mu-chlorido-bis({2-[(4-methoxyphenyl)-iminomethyl]pyridine-kappa N-2,N'] Mercury(II)

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Synthesis, Crystal Structure, and Antibacterial Activity of Di-mu-chlorido-bis({2-[(4-methoxyphenyl)-iminomethyl]pyridine-kappa N-2,N'] Mercury(II)

机译：Di-Mu-hollido-BIS的合成，晶体结构和抗菌活性（{2 - [（4-甲氧基苯基） - 咪唑-Kappa n-2，N']汞（II）

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A coordination polymer [Hg(L)Cl-2](n) consisting of HgCl2 and Schiff base bidentate ligand (4-methoxyphenyl) pyridine-2yl methyleneamine (L) was prepared and structurally characterized. Coordination compound has been characterized by infrared spectroscopy, UV-visible spectroscopy, elemental analysis, and single-crystal X-ray diffraction. The compound crystallizes in the monoclinic sp. gr. P2(1)/c with a = 9.3053(17), b = 7.1125(13), c = 20.708(4) angstrom, and beta = 80.208(4)degrees. In the 1D network structure, the mercury(II) ion adopts a HgN2Cl3 distorted square pyramid geometry. In this complex, one chlorine atom acts as bridging ligand connecting two adjacent mercury(II) ions, while the L ligand is coordinated to mercury(II) ion in a cyclic-bidentate fashion forming a five-membered metallocyclic ring. Antibacterial activity of the complex, ligand, and metal salt was tested against Gram-positive bacteria Staphylococcus aureus and Gram-negative bacteria Escherichia coli.

机译：制备由HGCl 2和Schiff基底座配体（4-甲氧基苯基）吡啶-200甲基氨基（L）组成的配位聚合物[Hg（1）Cl-2]（n）组成并在结构表征。协调化合物的特征在于红外光谱，UV可见光谱，元素分析和单晶X射线衍射。该化合物在单斜晶型中结晶。 GR。 P2（1）/ c具有A = 9.3053（17），B = 7.1125（13），C = 20.708（4）埃，β= 80.208（4）度。在1D网络结构中，汞（II）离子采用HGN2CL3扭曲的方形金字塔几何形状。在该络合物中，一种氯原子用作连接两个相邻的汞（II）离子的桥接配体，而L配体与形成五元茂金环环的环状双齿时的汞（II）离子配位。复合物，配体和金属盐的抗菌活性对革兰氏阳性细菌金黄色葡萄球菌和革兰氏阴性细菌大肠杆菌进行了测试。

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《Crystallography reports》 |2019年第7期|共4页
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机译：Di-Mu-hollido-BIS的合成，晶体结构和抗菌活性（{2 - [（4-甲氧基苯基） - 咪唑-Kappa n-2，N']汞（II）
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Synthesis, Crystal Structure, and Antibacterial Activity of Di-mu-chlorido-bis({2-[(4-methoxyphenyl)-iminomethyl]pyridine-kappa N-2,N'] Mercury(II)

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