Synthesis and Crystal Structure of Dibromido{2-[(4-tert-butylmethylphenyl)iminomethyl]pyridine-kappa N-2,N '}Zinc

Khalaj M.; Ghazanfarpour-Darjani M.; Seftejani F. B.; Lalegani A.

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Synthesis and Crystal Structure of Dibromido{2-[(4-tert-butylmethylphenyl)iminomethyl]pyridine-kappa N-2,N '}Zinc

机译：二溴化物{2 - [（4-叔丁基甲基苯基）咪啶-Kappa n-2，N'}锌的合成和晶体结构

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The title compound [Zn(dip) Br-2] was synthesized using the Schiff base bidentate ligand (E)-4-tert-butyl-N-(pyridine-2-ylmethylene) benzeneamine (dip) and zinc(II) bromide salts. It has been characterized by elemental analysis, X-ray diffraction, and optical spectroscopy. The X-ray diffraction analysis demonstrates that in this structure, the zinc(II) ion is located on an inversion center and exhibits a ZnN2Br2 tetrahedral geometry. In this structure the dip ligand is coordinated with zinc(II) ion in a cyclic-bidentate fashion forming a five-membered metallocyclic ring. The compound crystallizes in the monoclinic sp. gr. P2(1)/m with a = 9.2700(13)angstrom, b = 7.6128(11)angstrom, c = 12.3880(17)angstrom, and beta= 97.021(3)degrees.

机译：使用Schiff基底座配体（E）-4-叔丁基-N-（吡啶-2-基甲基）苯并氨基（浸渍）和锌（II）溴化锌合成标题化合物[Zn（DIP）BR-2] 。它的特征在于元素分析，X射线衍射和光学光谱。 X射线衍射分析表明，在该结构中，锌（II）离子位于倒置中心，并且表现出ZnN2BR2四面体几何形状。在该结构中，浸渍配体与锌（II）离子配位，以循环双齿时的形成五元核环环。该化合物在单斜晶型中结晶。 GR。 P2（1）/ m具有A = 9.2700（13）埃，B = 7.6128（11）埃，C = 12.3880（17）埃，β= 97.021（3）度。

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《Crystallography reports》 |2017年第7期|共3页
作者
Khalaj M.; Ghazanfarpour-Darjani M.; Seftejani F. B.; Lalegani A.;
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Islamic Azad Univ Buinzahra Branch Young Researchers &

Elite Club Buinzahra Iran;

Islamic Azad Univ Buinzahra Branch Young Researchers &

Elite Club Buinzahra Iran;

Islamic Azad Univ Buinzahra Branch Young Researchers &

Elite Club Buinzahra Iran;

Islamic Azad Univ Buinzahra Branch Young Researchers &

Elite Club Buinzahra Iran;

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正文语种 eng
中图分类晶体学;
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Synthesis and Crystal Structure of Dibromido{2-[(4-tert-butylmethylphenyl)iminomethyl]pyridine-kappa N-2,N '}Zinc

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