Controlled growth of lead oxide nanosheets, scrolled nanotubes, and nanorods

Shi L; Xu YM; Li Q

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Controlled growth of lead oxide nanosheets, scrolled nanotubes, and nanorods

机译：受控生长氧化铅纳米片，滚动纳米管和纳米棒

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PbO2 nanosheets, scrolled nanotubes, and nanorods have been selectively synthesized on lead foil with a convenient hydrothermal approach by simply modifying the reaction conditions. The presence of ammonia plays a key role in the preparation of PbO2 nanosheets, while the volume ratio of NH3 to H2O and reaction temperature have a significant influence on the shapes and sizes of the PbO2 product. The formation mechanism of the PbO2 nanostructures was discussed. The samples were characterized using X-ray powder diffraction, energy dispersive X-ray spectrometry, transmission electron microscopy, and scanning electron microscopy.

机译：通过简单地改变反应条件，通过方便的水热方法，在铅箔上选择性地合成了PbO2纳米片，涡旋纳米管和纳米棒。氨的存在在PbO2纳米片的制备中起着关键作用，而NH3与H2O的体积比和反应温度对PbO2产物的形状和尺寸有重要影响。讨论了PbO2纳米结构的形成机理。使用X射线粉末衍射，能量色散X射线光谱法，透射电子显微镜和扫描电子显微镜对样品进行表征。

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来源
《Crystal growth & design》 |2008年第10期|共5页
作者
Shi L; Xu YM; Li Q;
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正文语种 eng
中图分类晶体学;
关键词
NANOWIRES; NANOBELTS; DIOXIDE; PHOTOLUMINESCENCE; NANOCRYSTALS; MORPHOLOGY; SURFACE; PB3O4; PBO2; ZNO;

机译：纳米线;纳米带;二氧化物;光致发光;纳米晶体;形态学;表面;PB3O4;PBO2;ZNO;

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1. Controlled growth of lead oxide nanosheets, scrolled nanotubes, and nanorods [J] . Shi L, Xu YM, Li Q Crystal growth & design . 2008,第10期

机译：受控生长氧化铅纳米片，滚动纳米管和纳米棒
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Controlled growth of lead oxide nanosheets, scrolled nanotubes, and nanorods

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