Synthesis and crystal structure of (2-chloro-4-(phenylthio)phenyl) (3-methyl-1-phenyl-5-(phenylthio)-1H-pyrazol-4-yl)methanone

Sun G. -X.; Zhai Z. -W.; Sun Z. -H.; Tan C. -X.; Weng J. -Q.; Liu X. -H.

首页> 外文期刊>Journal of structural chemistry >Synthesis and crystal structure of (2-chloro-4-(phenylthio)phenyl) (3-methyl-1-phenyl-5-(phenylthio)-1H-pyrazol-4-yl)methanone

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Synthesis and crystal structure of (2-chloro-4-(phenylthio)phenyl) (3-methyl-1-phenyl-5-(phenylthio)-1H-pyrazol-4-yl)methanone

机译：（2-氯-4-（苯硫基）苯基）（3-甲基-1-苯基-5-（苯硫基）-1H-吡唑-4-基）的合成和晶体结构

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(2-Chloro-4-(phenylthio)phenyl)(3-methyl-1-phenyl-5-(phenylthio)-1H-pyrazol-4-yl)methanone was obtained by accident. In order to know the structure of this product, the compound was isolated by column chromatography and recrystallized from EtOH. The compound was characterized by X-ray diffraction. The compound crystallized in the triclinic space group P-1 with a = 9.909(2) , b = 11.824(2) , c = 13.056(3) , alpha = 63.309(3)A degrees, beta = 89.964(4)A degrees, gamma = 67.727(3)A degrees, V = 1237.7(4) (3), Z = 2 and R = 0.0414.

机译：（2-氯-4-（苯硫基）苯基）（3-甲基-1-苯基-5-（苯硫基）-1H-吡唑-4-基）通过意外获得甲基酮。为了了解该产品的结构，通过柱色谱法分离化合物并从EtOH中重结晶。该化合物的特征在于X射线衍射。用A = 9.909（2），B = 11.824（2），C = 13.056（3），Alpha = 63.309（3），α= 89.964（4）度，γ= 67.727（3）度，V = 1237.7（4）（3），Z = 2和R = 0.0414。

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来源
《Journal of structural chemistry》 |2017年第8期|共5页
作者
Sun G. -X.; Zhai Z. -W.; Sun Z. -H.; Tan C. -X.; Weng J. -Q.; Liu X. -H.;
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作者单位

Yancheng Inst Technol Sch Chem &

Chem Engn Yancheng Jiangsu Peoples R China;

Zhejiang Univ Technol Coll Chem Engn Hangzhou Zhejiang Peoples R China;

Zhejiang Univ Technol Coll Chem Engn Hangzhou Zhejiang Peoples R China;

Zhejiang Univ Technol Coll Chem Engn Hangzhou Zhejiang Peoples R China;

Zhejiang Univ Technol Coll Chem Engn Hangzhou Zhejiang Peoples R China;

Zhejiang Univ Technol Coll Chem Engn Hangzhou Zhejiang Peoples R China;

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原文格式 PDF
正文语种 eng
中图分类结构化学;
关键词
aryl sulfide; synthesis; crystal structure;

机译：芳硫醚;合成;晶体结构;

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Synthesis and crystal structure of (2-chloro-4-(phenylthio)phenyl) (3-methyl-1-phenyl-5-(phenylthio)-1H-pyrazol-4-yl)methanone

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