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首页> 外文期刊>Biomedical Chromatography: An International Journal Devoted to Research in Chromatographic Methodologies and Their Applications in the Biosciences >Quantitative determination of salidroside and specnuezhenide in the fruits of Ligustrum lucidum Ait by high performance liquid chromatography.
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Quantitative determination of salidroside and specnuezhenide in the fruits of Ligustrum lucidum Ait by high performance liquid chromatography.

机译：高效液相色谱法定量测定女贞子果实中的红景天苷和番木贼苷。

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摘要

An accurate RP-HPLC method for the quantitative determination of two water-soluble biologically active compounds, salidroside (p-hydroxyphenethyl-beta-D-glucoside) and specnuezhenide in the fruits of Ligustrum lucidum Ait (a crude drug in Chinese traditional medicine) was developed. The reversed-phase column was Nova-Pak C18, saturated with water before the injection of the samples and eluted with a mobile phase of methanol:water (4:6, v/v). The detection wavelength was 230 nm. The recoveries of the two compounds were 96.1 and 97.0%, respectively. The contents of salidroside and specnuezhenide in the fruits of Ligustrum lucidum Ait and two traditional Chinese patent medicines in which this crude drug was an important component, Erzhi Pills and Anshenbuxin Pills, were determined.
机译：准确的RP-HPLC方法用于定量测定女贞子（中药材中的一种）果实中的两种水溶性生物活性化合物红景天苷（对羟基苯乙基-β-D-D-葡萄糖苷）和番木贼苷。发达。反相色谱柱为Nova-Pak C18，在进样前先用水饱和，并用甲醇：水（4：6，v / v）的流动相洗脱。检测波长为230nm。两种化合物的回收率分别为96.1％和97.0％。测定了女贞子和两种以中草药为主要成分的中成药水果中的红景天苷和番木瓜内酯的含量，其中二至丸和安神补心丸为主要成分。

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