Crystal Growth Conditions of Types I and II Na–Si Clathrates by Evaporation of Na from a Na–Si–Sn Solution

Haruhiko Morito; Masashi Shimoda; Hisanori Yamane; Kozo Fujiwara

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Crystal Growth Conditions of Types I and II Na–Si Clathrates by Evaporation of Na from a Na–Si–Sn Solution

机译：通过从Na-Si-Sn溶液中蒸发Na和II型Na-Si Clathrates的晶体生长条件

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Single crystals of the type I clathrate Na₈Si₄₆ were synthesized by the evaporation of Na from a Na–Si–Sn solution (Na:Si:Sn = 6:2:1 molar ratio) at 723–873 K under an Ar atmosphere of 105 Pa. In the mixture of type I and type II clathrates prepared by heating at 773 K for 72 h, type I single crystals with sizes of up to 5 mm were found. A single phase of single crystals of the Na₂₄Si₁₃₆ type-II clathrate having a {111} crystal facet of about 2 mm on one side was obtained by heating at 873 K for 9 h.]]>

机译：<！[cdata [ src ='http://pubs.acs.org/appl/literatum/publisher/achs/journals/content/cgdefu/2018/cgdefu.2018.18.issue-1/acs.cgd.7b01342/ 20171227 /图像/介质/ CG-2017-013422_0005.gif“> I型Clathrate Na _{8 Si _{46 的单晶被Na从Na蒸发合成 -Si-Sn溶液（Na：Si：Sn = 6：2：1摩尔比）在10 5 pa的AR气氛下在723-873k。在I型和II型的混合物中通过在773 k下加热制备的Clathrates 72小时，发现I型单个晶体，尺寸可达5毫米。通过在873处加热获得，在一侧的Na _{24 / si和Si 136 型II族曲线的单个晶片的单相，具有约2mm的{111}晶章。 k为9小时]]]>}}}

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《Crystal growth & design》 |2018年第1期|共5页
作者
Haruhiko Morito; Masashi Shimoda; Hisanori Yamane; Kozo Fujiwara;
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作者单位

Institute for Materials Research and Institute of Multidisciplinary Research for Advanced Materials Tohoku University 2-1-1 Katahira Aoba-ku Sendai 980-8577 Japan;

Institute for Materials Research and Institute of Multidisciplinary Research for Advanced Materials Tohoku University 2-1-1 Katahira Aoba-ku Sendai 980-8577 Japan;

Institute for Materials Research and Institute of Multidisciplinary Research for Advanced Materials Tohoku University 2-1-1 Katahira Aoba-ku Sendai 980-8577 Japan;

Institute for Materials Research and Institute of Multidisciplinary Research for Advanced Materials Tohoku University 2-1-1 Katahira Aoba-ku Sendai 980-8577 Japan;

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中图分类晶体学;
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1. Crystal Growth Conditions of Types I and II Na–Si Clathrates by Evaporation of Na from a Na–Si–Sn Solution [J] . Haruhiko Morito, Masashi Shimoda, Hisanori Yamane, Crystal growth & design . 2018,第1期

机译：通过从Na-Si-Sn溶液中蒸发Na和II型Na-Si Clathrates的晶体生长条件
2. Na- Ga- Si type- I clathrate single crystals grown via Na evaporation using Na- Ga and Na- Ga- Sn fluxes [J] . Urushiyama Hironao, Morito Haruhiko, Yamane Hisanori, RSC Advances . 2018,第71期

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3. Na–Ga–Si type-I clathrate single crystals grown via Na evaporation using Na–Ga and Na–Ga–Sn fluxes [J] . Hironao Urushiyama, Haruhiko Morito, Hisanori Yamane, RSC Advances . 2018,第71期

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Crystal Growth Conditions of Types I and II Na–Si Clathrates by Evaporation of Na from a Na–Si–Sn Solution

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