A convenient procedure for the synthesis of racemic syn-1,2-diarylethane-1,2- diols by osmate catalyzed dihydroxylation of trans-stilbenes facilitated by Troger base

Sakilam Satishkumar; Mariappan Periasamy

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A convenient procedure for the synthesis of racemic syn-1,2-diarylethane-1,2- diols by osmate catalyzed dihydroxylation of trans-stilbenes facilitated by Troger base

机译：一种由Troger碱促进的，通过膦酸酯催化反式-对苯二甲酸酯的二羟基化合成外消旋的syn-1,2-二芳基乙烷-1,2-二醇的便捷方法

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摘要

Racemic (dl) mixture of syn-1,2-diarylethane-1,2-diols are prepared from the corresponding substituted trans-stilbenes using osmate catalyzed dihydroxylation facilitated by racemic Troger base under ambient conditions.

机译：在环境条件下，由外消旋Troger碱促进的由膦酸酯催化的二羟基化反应，由相应的取代的反式-对苯二甲酸酯制备了顺式1,2-二芳基乙烷-1,2-二醇的外消旋（dl）混合物。

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《Indian Journal of Chemistry, Section B. Organic Including Medicinal》 |2008年第7期|共4页
作者
Sakilam Satishkumar; Mariappan Periasamy;
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正文语种 eng
中图分类化学;
关键词
Troger base; syn-1; 2-dipls; trans-stilbenes; racemic dihydroxylation; potasium osmate (VI) dihydrate;

机译：Troger碱;syn-1;2-dipls;反式-斯蒂苯酯;外消旋二羟基化;二水合酸钾（VI）;

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1. A convenient procedure for the synthesis of racemic syn-1,2-diarylethane-1,2- diols by osmate catalyzed dihydroxylation of trans-stilbenes facilitated by Troger base [J] . Sakilam Satishkumar, Mariappan Periasamy Indian Journal of Chemistry, Section B. Organic Including Medicinal . 2008,第7期

机译：一种由Troger碱促进的，通过膦酸酯催化反式-对苯二甲酸酯的二羟基化合成外消旋的syn-1,2-二芳基乙烷-1,2-二醇的便捷方法
2. One-pot synthesis of enantiopure syn-1,3-diacetates from racemic syn/anti mixtures of 1,3-diols by dynamic kinetic asymmetric transformation [J] . Edin M, Steinreiber J, Backvall JE Proceedings of the National Academy of Sciences of the United States of America . 2004,第16期

机译：通过动态动力学不对称转化从1,3-二醇的外消旋式正/反混合物一锅合成对映体纯-1,3-二乙酸酯
3. A rare case of facial selectivity inversion for Sharpless asymmetric dihydroxylation in a series of structurally homogeneous substrates:synthesis of non-racemic 3-(nitrophenoxy)-propane-1,2-diols [J] . Zemfira A. Bredikhina, Alexey V. Kurenkov, Olga A. Antonovich, Tetrahedron, Asymmetry: The International Journal for Repid Publication on all Aspects of Asymmetry in Orgainc, Inorganic, Organometallic, Physical and Bio-Organic Chemistry . 2014,第13a14期

机译：在一系列结构均质的底物中发生Sharpless不对称二羟基化反应的面部选择性反转的罕见情况：非外消旋3-（硝基苯氧基）-丙烷-1,2-二醇的合成
4. Synthesis of Polycarbonate Diol Catalyzed by Metal-Organic Framework Based on Zn~(2+) and Terephthalic Acid [C] . Liping Wang, Gongying Wang, Fan Wang, ICCMME 2012 . 2013

机译：基于Zn〜（2+）和对苯二甲酸的金属 - 有机骨架催化合成聚碳酸酯二醇
5. Cu(II) Complexes of 4-(1E)-N-{2-(Z)-Benzylidene-aminoethyl}ethanimidoylbenzene-13-diol Schiff Base: Synthesis Spectroscopic In-Vitro Antioxidant Antifungal and Antibacterial Studies [O] . Ikechukwu P. Ejidike 2018

机译：4-（1E）-N- {2-（Z）-苄叉基-氨基乙基}乙亚氨基酰基苯-13-二醇席夫碱的Cu（II）配合物：合成光谱体外抗氧化剂抗真菌和抗菌研究
6. One-pot synthesis of enantiopure syn-1,3-diacetates from racemic syn/anti mixtures of 1,3-diols by dynamic kinetic asymmetric transformation [O] . Edin, Michaela, Steinreiber, Johannes, Bäckvall, Jan-E. 2004

机译：通过动态动力学不对称转化从1,3-二醇的外消旋式正/反混合物一锅合成对映体纯-1,3-二乙酸酯

A convenient procedure for the synthesis of racemic syn-1,2-diarylethane-1,2- diols by osmate catalyzed dihydroxylation of trans-stilbenes facilitated by Troger base

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