Spectral and single crystal X-ray diffraction studies of (E)-4-chloro-N (2-hydroxy-benzylidene)benzohydrazide

A Padmaja; Aliya Begum; P Ragavaiah

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Spectral and single crystal X-ray diffraction studies of (E)-4-chloro-N (2-hydroxy-benzylidene)benzohydrazide

机译：（E）-4-氯-N（2-羟基-亚苄基）苯甲酰肼的光谱和单晶X射线衍射研究

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(E)-4-Chloro-N(2-hydroxybenzylidene)benzohydrazide is synthesized and characterized by elemental analysis, IR, ~1H NMR, ~(13)C NMR, DEPT and mass spectral studies. The structure and. types of hydrogen bonding present in crystalline form of title compound are envisaged from single crystal X-ray diffraction studies. The topological analysis of hydrogen bonds indicates both inter and intramolecular hydrogen bonding. The presence of water molecule in crystal structure indicates mono hydrated form of the title compound.

机译：（E）-4-氯-N（2-羟基亚苄基）苯甲酰肼的合成和表征方法包括元素分析，IR，〜1H NMR，〜（13）C NMR，DEPT和质谱研究。结构和。根据单晶X射线衍射研究，设想了以标题化合物的结晶形式存在的氢键的类型。氢键的拓扑分析表明分子间和分子内氢键均存在。晶体结构中水分子的存在表明标题化合物的单水合形式。

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《Indian Journal of Chemistry, Section B. Organic Including Medicinal》 |2011年第3期|共4页
作者
A Padmaja; Aliya Begum; P Ragavaiah;
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正文语种 eng
中图分类化学;
关键词
(E)-4-Chloro-B'(2-hydroxybenzylidene)benzohydra-zide; hydrogen bonding; X-ray diffraction; hydrated form; IR; ~1H NMR; ~(13)C NMR; DEPT;

机译：（E）-4-氯-B'（2-羟基亚苄基）苯甲酰肼;氢键;X射线衍射;水合物;IR;〜1H NMR;〜（13）C NMR;DEPT;

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1. Spectral and single crystal X-ray diffraction studies of (E)-4-chloro-N (2-hydroxy-benzylidene)benzohydrazide [J] . A Padmaja, Aliya Begum, P Ragavaiah Indian Journal of Chemistry, Section B. Organic Including Medicinal . 2011,第3期

机译：（E）-4-氯-N（2-羟基-亚苄基）苯甲酰肼的光谱和单晶X射线衍射研究
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Spectral and single crystal X-ray diffraction studies of (E)-4-chloro-N (2-hydroxy-benzylidene)benzohydrazide

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