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首页> 外文期刊>Food and Chemical Toxicology: An International Journal Published for the British Industrial Biological Research >Detection of furan levels in select Chinese foods by solid phase microextraction-gas chromatography/mass spectrometry method and dietary exposure estimation of furan in the Chinese population
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Detection of furan levels in select Chinese foods by solid phase microextraction-gas chromatography/mass spectrometry method and dietary exposure estimation of furan in the Chinese population

机译:固相微萃取-气相色谱/质谱法检测某些中国食品中的呋喃水平,并通过膳食估算中国人群中的呋喃

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摘要

In this study, a solid phase microextraction-gas chromatography/mass spectrometry (SPMEGC/MS) method was developed to detection the levels of furan in 191 selected food products obtained from the Chinese markets. The performance of the analysis method was evaluated by some quality parameters such as limit of detection (LOD), limit of quantification (LOQJ, linearity, recovery, and runto-run (n = 6) and day-to-day (n = 18) precisions. The LOD and the LOQ. of the method were 0.059 ng/g and 0.175 ng/ g, respectively. The recovery of the method in fruit juice, canned jam, and infant formula ranged from 93.25% to 104.69%. The results from this study showed that furan was detected in almost all analyzed samples. Furan contents in different food samples varied greatly according to the raw materials and processing conditions. The higher contents of furan were detected in traditional Chinese liquor (61.63 ng/g), coffee (71.36 ng/g), tea (68.28 ng/g) and pickle (85.63 ng/g). The dietary intake of furan was estimated to be 0.093 ug/kg b.w.t/day in adults and 0.333mug/kg b.w.t/day in infants at 6 months. Further studies are needed to reveal other sources of dietary furan exposure.
机译:在这项研究中,开发了一种固相微萃取-气相色谱/质谱(SPMEGC / MS)方法来检测从中国市场获得的191种精选食品中的呋喃含量。分析方法的性能通过一些质量参数进行评估,例如检出限(LOD),定量限(LOQJ,线性,回收率和连续运行(n = 6)和日常(n = 18)方法的LOD和LOQ。分别为0.059 ng / g和0.175 ng / g,在果汁,果酱罐头和婴儿配方食品中的回收率在93.25%至104.69%之间。这项研究表明,几乎所有分析样品中都检出了呋喃,不同食品样品中的呋喃含量因原料和加工条件的不同而有很大差异,在传统白酒,咖啡,咖啡中检出的呋喃含量较高。 (71.36 ng / g),茶(68.28 ng / g)和泡菜(85.63 ng / g),成人的呋喃饮食摄入量估计为0.093 ug / kg bwt /天,而成人的饮食摄入量为0.333mug / kg bwt /天。六个月大的婴儿,还需要进一步研究以揭示膳食中呋喃暴露的其他来源。

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