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Survey of aflatoxins and ochratoxin a contamination in food products imported in Italy.

机译:黄曲霉毒素和曲霉毒素在意大利进口食品中的污染情况调查。

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摘要

In this study the levels of aflatoxins (AF B1, B2, G1 and G2) and ochratoxin A (OTA) were monitored in several food products imported in Italy with a high contamination risk. A total of 345 samples were collected from the Maritime Authority of Salerno Customs Port during the period from January 2008 to December 2009 and analyzed by immunoaffinity chromatography as clean-up, high performance liquid chromatography with fluorescence detection for quantification and tandem mass spectrometry for confirmation. The analytical methods were validated on different food matrices and meet the performance criteria set by EC Regulation No. 401/2006 for mycotoxin analysis. The results obtained in this survey showed that 7% of the total samples contained detectable levels of AFs and OTA, and 1.2% had AFs concentrations exceeding the maximum limits set by EU regulation. OTA was the most prevalent mycotoxin, with an incidence of 17.6% of samples analyzed for OTA. The highest detected levels were 23.70 mug kg--1 of OTA in a green coffee sample and 70.69 mug kg--1 of AFs in an apricot kernels sample. Among the food products analyzed, hazelnuts paste and dried vine fruits were the commodities mainly contaminated with AFs and OTA, respectively.
机译:在这项研究中,黄曲霉毒素的水平(AF B 1 ,B 2 ,G 1 和G 2 )和在意大利进口的几种污染风险较高的食品中检测到曲霉毒素A(OTA)。从2008年1月至2009年12月期间,从萨勒诺海关港口海事管理局收集了345个样品,并通过免疫亲和色谱法进行了分析,如净化,高效液相色谱法和荧光检测(用于定量​​)以及串联质谱法进行了确认。该分析方法在不同的食品基质上得到验证,并符合EC法规401/2006所设定的用于霉菌毒素分析的性能标准。该调查获得的结果表明,总样品中有7%的AF和OTA含量可检测到,而1.2%的AF含量超过了欧盟规定的最大限量。 OTA是最普遍的霉菌毒素,分析过的OTA样本中有17.6%的发生率。最高检测到的水平是生咖啡样品中的OTA为23.70杯kg -1 ,杏仁样品中的AFs为70.69杯kg -1 。在分析的食品中,榛子酱和葡萄干是分别被AF和OTA污染的商品。

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