DDQ-mediated synthesis of functionalized unsymmetrical disulfanes

Musiejuk Mateusz; Klucznik Tomasz; Rachon Janusz; Witt Dariusz

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DDQ-mediated synthesis of functionalized unsymmetrical disulfanes

机译：DDQ介导的功能化不对称二硫烷的合成

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We developed a simple and efficient method for the synthesis of functionalized unsymmetrical disulfanes under mild conditions in good yields. The designed method is based on the reaction of bis(5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphorinan-2-yl) disulfane with thiols in the presence of 2,3-dichloro-5,6-dicyanobenzoquinone (DDQ). The developed method allows the preparation of unsymmetrical disulfanes bearing additional hydroxy, carboxy, or amino functionalities.

机译：我们开发了一种简单有效的方法，可在温和条件下以高收率合成功能化的不对称二硫烷。设计的方法基于在2,3-二氯-5,6-存在下双（5,5-二甲基-2-硫代氧-1,3,2-二氧杂磷酰氨基-2-基）二硫醚与硫醇的反应双氰基苯醌（DDQ）。所开发的方法允许制备带有额外羟基，羧基或氨基官能团的不对称二硫烷。

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《RSC Advances》 |2015年第40期|共5页
作者
Musiejuk Mateusz; Klucznik Tomasz; Rachon Janusz; Witt Dariusz;
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正文语种 eng
中图分类化学;
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1. DDQ-mediated synthesis of functionalized unsymmetrical disulfanes [J] . Musiejuk Mateusz, Klucznik Tomasz, Rachon Janusz, RSC Advances . 2015,第40期

机译：DDQ介导的功能化不对称二硫烷的合成
2. Synthesis of unsymmetrical disulfanes bearing 1,2,4-triazine scaffold and their in vitro screening towards anti-breast cancer activity [J] . Branowska Danuta, Lawecka Justyna, Sobiczewski Mariusz, Monatshefte fur Chemie . 2018,第8期

机译：非对称二丁烯含有1,2,4-三嗪支架及其对抗乳腺癌活性的体外筛选的非对称硫胺
3. Oxidative cross S-H/S-H coupling: selective synthesis of unsymmetrical aryl tert-alkyl disulfanes [J] . Jiwen Yuan, Chao Liu, Aiwen Lei Organic Chemistry Frontiers . 2015,第6期

机译：氧化交叉S-H / S-H偶联：不对称芳基叔烷基二硫醚的选择性合成
4. Study on Photoresponsive Functional Materials with Efficient Synthesis, Properties of a Novel Unsymmetrical Photochromic Diarylethene [C] . Hongjing Jia, Shouzhi Pu International Conference on Intelligent Materials, Applied Mechanics and Design Science . 2013

机译：具有高效合成的光反应功能性材料，新型非对称光致变色二丙烯烯的性质
5. An application of the intramolecular Heck reaction: A new strategy in the synthesis of Hasubanan alkaloids. Preparation of unsymmetrical biaryls via the Stille cross-coupling reaction: Synthesis of highly functional intermediates towards the synthesis of vindoline. [D] . Frank, Anthony Joseph. 2002

机译：分子内Heck反应的应用：合成Hasubanan生物碱的新策略。通过Stille交叉偶联反应制备不对称的联芳基：合成高功能性中间体，合成长春新碱。
6. Synthesis of unsymmetrical disulfanes bearing 124-triazine scaffold and their in vitro screening towards anti-breast cancer activity [O] . Danuta Branowska, Justyna Ławecka, Mariusz Sobiczewski, -1

机译：带有124-三嗪骨架的不对称二硫烷的合成及其体外抗乳腺癌活性筛选
7. Phthalimide-Carried Disulfur Transfer To Synthesize Unsymmetrical Disulfanes via Copper Catalysis [O] . -1

机译：邻苯二甲酰酰亚胺携带的无比转移以通过铜催化合成非对称二硫胺醛

DDQ-mediated synthesis of functionalized unsymmetrical disulfanes

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